Technology Process of C30H49N5O5
There total 6 articles about C30H49N5O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
2-hydroxypyridin; triethylamine;
at 80 - 90 ℃;
for 30h;
Product distribution / selectivity;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: magnesium; ethylene dibromide / 2-methyltetrahydrofuran / 60 - 65 °C
1.2: 0.25 h / 10 °C
2.1: N-Bromosuccinimide; phosphoric acid / water; tetrahydrofuran / 5 °C
3.1: sodium azide; Aliquat 336 / water / 48 h / 75 - 80 °C
4.1: triethylamine; 2-hydroxypyridin / 30 h / 80 - 90 °C
With
2-hydroxypyridin; N-Bromosuccinimide; sodium azide; phosphoric acid; Aliquat 336; magnesium; ethylene dibromide; triethylamine;
In
tetrahydrofuran; 2-methyltetrahydrofuran; water;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: magnesium; ethylene dibromide / 2-methyltetrahydrofuran / 60 - 65 °C
1.2: 0.25 h / 10 °C
2.1: N-Bromosuccinimide; phosphoric acid / water; tetrahydrofuran / 5 °C
3.1: sodium azide; Aliquat 336 / water / 48 h / 75 - 80 °C
4.1: triethylamine; 2-hydroxypyridin / 30 h / 80 - 90 °C
With
2-hydroxypyridin; N-Bromosuccinimide; sodium azide; phosphoric acid; Aliquat 336; magnesium; ethylene dibromide; triethylamine;
In
tetrahydrofuran; 2-methyltetrahydrofuran; water;