trans-3-[(tert-butoxycarbonyl)amino]cyclobutyl 4-nitrobenzoate

Base Information Edit

Chemical Name:trans-3-[(tert-butoxycarbonyl)amino]cyclobutyl 4-nitrobenzoate
CAS No.:871014-16-3
Molecular Formula:C₁₆H₂₀N₂O₆
Molecular Weight:336.345
Hs Code.:
Mol file:871014-16-3.mol

Synonyms:trans-3-[(tert-butoxycarbonyl)amino]cyclobutyl 4-nitrobenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-3-[(tert-butoxycarbonyl)amino]cyclobutyl 4-nitrobenzoate Edit

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of trans-3-[(tert-butoxycarbonyl)amino]cyclobutyl 4-nitrobenzoate

There total 2 articles about trans-3-[(tert-butoxycarbonyl)amino]cyclobutyl 4-nitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 389890-43-1
tert-butyl (1,3-cis)-N-(3-hydroxycyclobutyl)carbamate

: 62-23-7
4-nitro-benzoic acid

: 871014-16-3
trans-3-[(tert-butoxycarbonyl)amino]cyclobutyl 4-nitrobenzoate

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 48h; Cooling with ice;

Reference yield:

: 154748-49-9
3-(tert-butyloxycarbonylamino)cyclobutan-1-one

: 871014-16-3
trans-3-[(tert-butoxycarbonyl)amino]cyclobutyl 4-nitrobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: L-Selectride / tetrahydrofuran / 1 h / -78 °C

2: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 48 h / 20 °C / Cooling with ice

With di-isopropyl azodicarboxylate; L-Selectride; triphenylphosphine; In tetrahydrofuran;