C₁₆H₁₉NOSi

Base Information

• Chemical Name: C₁₆H₁₉NOSi
• CAS No.: 1450667-18-1
• Molecular Formula: C₁₆H₁₉NOSi
• Molecular Weight: 269.418
• Mol file: 1450667-18-1.mol

Synonyms:C₁₆H₁₉NOSi

Chemical Property of C₁₆H₁₉NOSi

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₁₆H₁₉NOSi

There total 4 articles about C₁₆H₁₉NOSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C16H17N3OSi (1450667-14-7) → C16H19NOSi (1450667-18-1)

Guidance literature:

With tin(ll) chloride; In methanol; Inert atmosphere;

DOI:10.1016/j.tetlet.2013.07.001

Reference yield:

C16H16OSi → C16H19NOSi (1450667-18-1)

Guidance literature:

Multi-step reaction with 2 steps

1: (1R,2R) N,N′-bis(3,5-di-tertbutylsalicylidene)-1,2-cyclohexanediamino chromium(III) chloride / diethyl ether / 0.25 h / 20 °C

2: tin(ll) chloride / methanol / Inert atmosphere

With (1R,2R) N,N′-bis(3,5-di-tertbutylsalicylidene)-1,2-cyclohexanediamino chromium(III) chloride; tin(ll) chloride; In methanol; diethyl ether;

DOI:10.1016/j.tetlet.2013.07.001

Reference yield:

C16H17ClOSi (1450667-16-9) → C16H19NOSi (1450667-18-1)

Guidance literature:

Multi-step reaction with 3 steps

1: (1R,2R) N,N′-bis(3,5-di-tertbutylsalicylidene)-1,2-cyclohexanediamino chromium(III) chloride / diethyl ether / 0.25 h / -70 °C

2: (1R,2R) N,N′-bis(3,5-di-tertbutylsalicylidene)-1,2-cyclohexanediamino chromium(III) chloride / diethyl ether / 0.25 h / 20 °C

3: tin(ll) chloride / methanol / Inert atmosphere

With (1R,2R) N,N′-bis(3,5-di-tertbutylsalicylidene)-1,2-cyclohexanediamino chromium(III) chloride; tin(ll) chloride; In methanol; diethyl ether;

DOI:10.1016/j.tetlet.2013.07.001

upstream raw materials:

C₁₆H₁₇N₃OSi

C₁₉H₂₅N₃OSi₂

C₁₆H₁₇ClOSi

Downstream raw materials:

(2S,3R)-2-amino-1,3,4-butanetriol

C₂₃H₂₃NO₂Si

Refernces