Technology Process of C29H27F2IN3O9P
There total 6 articles about C29H27F2IN3O9P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
1-methyl-1H-imidazole;
In
tetrahydrofuran;
at 20 ℃;
for 24h;
Inert atmosphere;
DOI:10.1016/j.bmc.2011.05.037
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: lithium tri-t-butoxyaluminum hydride / tetrahydrofuran; diethyl ether / 1 h / -78 °C / Inert atmosphere
2.1: triethylamine / dichloromethane / 18 h / 0 - 20 °C / Inert atmosphere
3.1: trimethylsilyl trifluoromethanesulfonate / 1,1-dichloroethane / 10 h / 90 - 100 °C / Inert atmosphere
3.2: 20 °C
4.1: sodium methylate / methanol / 20 °C / Inert atmosphere
4.2: Amberlite
5.1: 1-methyl-1H-imidazole / tetrahydrofuran / 24 h / 20 °C / Inert atmosphere
With
1-methyl-1H-imidazole; trimethylsilyl trifluoromethanesulfonate; sodium methylate; lithium tri-t-butoxyaluminum hydride; triethylamine;
In
tetrahydrofuran; methanol; diethyl ether; 1,1-dichloroethane; dichloromethane;
DOI:10.1016/j.bmc.2011.05.037
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: triethylamine / dichloromethane / 18 h / 0 - 20 °C / Inert atmosphere
2.1: trimethylsilyl trifluoromethanesulfonate / 1,1-dichloroethane / 10 h / 90 - 100 °C / Inert atmosphere
2.2: 20 °C
3.1: sodium methylate / methanol / 20 °C / Inert atmosphere
3.2: Amberlite
4.1: 1-methyl-1H-imidazole / tetrahydrofuran / 24 h / 20 °C / Inert atmosphere
With
1-methyl-1H-imidazole; trimethylsilyl trifluoromethanesulfonate; sodium methylate; triethylamine;
In
tetrahydrofuran; methanol; 1,1-dichloroethane; dichloromethane;
DOI:10.1016/j.bmc.2011.05.037