Technology Process of (E)-2-methyl-1-phenyl-4-(trifluoromethyl)penta-1,4-dien-3-one
There total 1 articles about (E)-2-methyl-1-phenyl-4-(trifluoromethyl)penta-1,4-dien-3-one which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
2-bromo-3,3,3-trifluoropropene;
With
n-butyllithium; boron trifluoride diethyl etherate;
In
diethyl ether; hexane;
at -100 ℃;
for 0.166667h;
Inert atmosphere;
N,N-dimethyl methyl-2 phenyl-3 propene-2 amide;
In
diethyl ether; hexane;
at -100 - -50 ℃;
for 2h;
Inert atmosphere;
With
water;
In
diethyl ether; hexane;
pH=7;
aq. phosphate buffer;
DOI:10.1002/asia.201000139
- Guidance literature:
-
With
trimethylsilyl trifluoromethanesulfonate;
In
1,1,1,3',3',3'-hexafluoro-propanol;
at 20 ℃;
for 0.166667h;
Inert atmosphere;
DOI:10.1002/asia.201000139