1-BROMO-3,5,5-TRIMETHYL HEXANE

Base Information

• Chemical Name: 1-BROMO-3,5,5-TRIMETHYL HEXANE
• CAS No.: 50915-80-5
• Molecular Formula: C9H19 Br
• Molecular Weight: 207.154
• Hs Code.: 2903399090
• Mol file: 50915-80-5.mol

Synonyms:1-Bromo-3,5,5-trimethylhexane;3,5,5-Trimethylhexyl bromide

Chemical Property of 1-BROMO-3,5,5-TRIMETHYL HEXANE

Chemical Property:

• Vapor Pressure: 0.553mmHg at 25°C
• Refractive Index: 1.451
• Boiling Point: 196.7 °C at 760 mmHg
• Flash Point: 59 °C
• PSA: 0.00000
• Density: 1.086 g/cm³
• LogP: 3.84370

Purity/Quality:

99% ^*data from raw suppliers

1-Bromo-3,5,5-trimethylhexane 99% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-BROMO-3,5,5-TRIMETHYL HEXANE

There total 2 articles about 1-BROMO-3,5,5-TRIMETHYL HEXANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.1%

isononanol (3452-97-9,140237-84-9,140237-85-0) → 1-bromo-3,5,5-trimethylhexane (50915-80-5)

Guidance literature:

With sulfuric acid; hydrogen bromide; In water; at 120 ℃; for 3h;

DOI:10.1021/ja804415b

Reference yield:

→ 1-bromo-3,5,5-trimethylhexane (50915-80-5)

Guidance literature:

/BRN= 773688/;

Reference yield: 78.0%

1-bromo-3,5,5-trimethylhexane (50915-80-5) + 1-amino-3-methylbenzene (108-44-1) → N,N-di-(3,5,5-trimethylhexyl)-m-toluidine

Guidance literature:

With sodium hydrogencarbonate; In 1-methyl-pyrrolidin-2-one; at 100 - 140 ℃; for 120h; Temperature; Time;

upstream raw materials:

isononanol

Downstream raw materials:

2,2,4-trimethylhexane

(1,1,4,6,6-pentamethylheptyl)benzene

1-(3,5,5-trimethylhexyl)-cyclopropene

pinacol 1-(phenylthio)-t-BuCH₂CH(CH₃)CH₂CH₂CH-1-boronate

Refernces

• 1、 -. "Ammonium cation-containing organic salt". Paragraph 0044; 0045. . Retrieved 2017/01/31.
• 2、 Raymond, Jeffery E.,Bhaskar, Ajit,Goodson, Theodore,Makiuchi, Naoyuki,Ogawa, Kazuya,Kobuke, Yoshiaki. "Synthesis and two-photon absorption enhancement of porphyrin macrocycles". supporting information; experimental part. p. 17212 - 17213. Retrieved 2009/07/11.