tris (3-ethyl phenyl sulfonate) phosphine

Base Information

• Chemical Name: tris (3-ethyl phenyl sulfonate) phosphine
• CAS No.: 135265-27-9
• Molecular Formula: C₂₄H₂₇O₉PS₃
• Molecular Weight: 586.645
• Mol file: 135265-27-9.mol

Synonyms:tris (3-ethyl phenyl sulfonate) phosphine

Chemical Property of tris (3-ethyl phenyl sulfonate) phosphine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of tris (3-ethyl phenyl sulfonate) phosphine

There total 2 articles about tris (3-ethyl phenyl sulfonate) phosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

tris (3-ethyl phenyl sulfonate) phosphine oxide (135265-26-8) → tris (3-ethyl phenyl sulfonate) phosphine (135265-27-9)

Guidance literature:

With trichlorosilane; In tetrahydrofuran; toluene; for 22h; Heating;

DOI:10.1080/00397919108016775

Reference yield:

tris (3-sulfonatophenyl) phosphine oxide, triacid (96723-93-2) → tris (3-ethyl phenyl sulfonate) phosphine (135265-27-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) Ag₂CO₃, aq. aerosol OT / 1.) 25 deg C, 24 h, 2.) toluene, reflux, 24 h

2: 89 percent / SiHCl₃ / toluene; tetrahydrofuran / 22 h / Heating

With aerosol OT; trichlorosilane; silver carbonate; In tetrahydrofuran; toluene;

DOI:10.1080/00397919108016775

Reference yield: 66.0%

tris (3-ethyl phenyl sulfonate) phosphine (135265-27-9) → trisodium tris(3-sulfophenyl)phosphine (63995-70-0)

Guidance literature:

With sodium bromide; In water; acetone; for 48h; Ambient temperature;

DOI:10.1080/00397919108016775

upstream raw materials:

tris (3-ethyl phenyl sulfonate) phosphine oxide

tris (3-sulfonatophenyl) phosphine oxide, triacid

Downstream raw materials:

trisodium tris(3-sulfophenyl)phosphine

methyl di (3-sulfonatophenyl) phosphine oxide, diacid

methyl di (3-ethyl phenyl sulfonate) phosphine

methyl di (3-ethyl phenyl sulfonate) phosphine oxide

Refernces