Technology Process of Carbamic acid, [2-amino-1-(methoxymethyl)-2-oxoethyl]-, 1,1-dimethylethyl
There total 7 articles about Carbamic acid, [2-amino-1-(methoxymethyl)-2-oxoethyl]-, 1,1-dimethylethyl which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
4-methyl-morpholine; ammonia; isobutyl chloroformate;
Yield given. Multistep reaction;
1.) THF, -15 deg C. 15 min, 2.) THF, -15 deg C, 10 min, warm to room temp. over 30 min;
DOI:10.1021/jo961408a
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 90 percent / H2 / Pd/C / methanol / 1 h / 760 Torr
2: 1.) N-methylmorpholine, isobutyl chloroformate, 2.) NH3 / 1.) THF, -15 deg C. 15 min, 2.) THF, -15 deg C, 10 min, warm to room temp. over 30 min
With
4-methyl-morpholine; ammonia; hydrogen; isobutyl chloroformate;
palladium on activated charcoal;
In
methanol;
DOI:10.1021/jo961408a