(2Z)-2-(3,4-diisopropoxy phenyl)-3-{4-[(11-hydroxyundecyl)oxy]-3-methoxyphenyl}prop-2-enenitrile

Base Information

• Chemical Name: (2Z)-2-(3,4-diisopropoxy phenyl)-3-{4-[(11-hydroxyundecyl)oxy]-3-methoxyphenyl}prop-2-enenitrile
• CAS No.: 1425539-72-5
• Molecular Formula: C₃₃H₄₇NO₅
• Molecular Weight: 537.74
• Mol file: 1425539-72-5.mol

Synonyms:(2Z)-2-(3,4-diisopropoxy phenyl)-3-{4-[(11-hydroxyundecyl)oxy]-3-methoxyphenyl}prop-2-enenitrile

Chemical Property of (2Z)-2-(3,4-diisopropoxy phenyl)-3-{4-[(11-hydroxyundecyl)oxy]-3-methoxyphenyl}prop-2-enenitrile

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (2Z)-2-(3,4-diisopropoxy phenyl)-3-{4-[(11-hydroxyundecyl)oxy]-3-methoxyphenyl}prop-2-enenitrile

There total 5 articles about (2Z)-2-(3,4-diisopropoxy phenyl)-3-{4-[(11-hydroxyundecyl)oxy]-3-methoxyphenyl}prop-2-enenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.3%

4-[(11-hydroxyundecyl)oxy]-3-methoxybenzaldehyde (1166992-10-4) + 2-(3,4-(diisopropoxy)phenyl)-acetonitrile (69769-47-7) → (2Z)-2-(3,4-diisopropoxy phenyl)-3-{4-[(11-hydroxyundecyl)oxy]-3-methoxyphenyl}prop-2-enenitrile (1425539-72-5)

Guidance literature:

With potassium tert-butylate; In tert-butyl methyl ether; at 54 ℃; for 62h;

Reference yield:

4-[(11-hydroxyundecyl)oxy]-3-methoxybenzaldehyde (1166992-10-4) + potassium tert-butylate (865-47-4) → (2Z)-2-(3,4-diisopropoxy phenyl)-3-{4-[(11-hydroxyundecyl)oxy]-3-methoxyphenyl}prop-2-enenitrile (1425539-72-5)

Guidance literature:

With hydrogenchloride; In tert-butyl methyl ether; water;

Reference yield:

1-Bromo-11-hydroxyundecane (1611-56-9) → (2Z)-2-(3,4-diisopropoxy phenyl)-3-{4-[(11-hydroxyundecyl)oxy]-3-methoxyphenyl}prop-2-enenitrile (1425539-72-5)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide; water

2: hydrogenchloride / water; tert-butyl methyl ether

With hydrogenchloride; potassium carbonate; In tert-butyl methyl ether; water; N,N-dimethyl-formamide;

upstream raw materials:

4-[(11-hydroxyundecyl)oxy]-3-methoxybenzaldehyde

potassium tert-butylate

1-Bromo-11-hydroxyundecane

vanillin

Refernces

• 1、 -. "PHOTOREACTIVE COMPOUNDS". Page/Page column. . Retrieved 2014/07/22.