C₂₂H₁₄N₂O₉

Base Information

• Chemical Name: C₂₂H₁₄N₂O₉
• CAS No.: 1391926-99-0
• Molecular Formula: C₂₂H₁₄N₂O₉
• Molecular Weight: 450.361
• Mol file: 1391926-99-0.mol

Synonyms:C₂₂H₁₄N₂O₉

Chemical Property of C₂₂H₁₄N₂O₉

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₂H₁₄N₂O₉

There total 6 articles about C₂₂H₁₄N₂O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

6-carboxylic benzo[c]isoxazol-3(1H)-one (31499-93-1) + 1-phenyl 2-nitrosoterephthalate (1391926-97-8) → C22H14N2O9 (1391926-99-0)

Guidance literature:

for 2h; Inert atmosphere; aq. phosphate buffer;

DOI:10.1002/anie.201201812

Reference yield:

L-Cysteine (52-90-4) + 1-phenyl 2-nitrosoterephthalate (1391926-97-8) → 6-carboxylic benzo[c]isoxazol-3(1H)-one (31499-93-1) + C14H11NO5 + C22H14N2O9 (1391926-99-0) + 3-aminoterephthalic acid (10312-55-7)

Guidance literature:

Inert atmosphere; aq. phosphate buffer;

DOI:10.1002/anie.201201812

Reference yield:

1-phenyl 2-aminoterephthalate (1391926-96-7) → C22H14N2O9 (1391926-99-0)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium peroxymonosulfate / dichloromethane; water / 23 h / Inert atmosphere

2: 2 h / Inert atmosphere; aq. phosphate buffer

With potassium peroxymonosulfate; In dichloromethane; water;

DOI:10.1002/anie.201201812

upstream raw materials:

1-phenyl 2-nitrosoterephthalate

6-carboxylic benzo[c]isoxazol-3(1H)-one

L-Cysteine

1-phenyl 2-aminoterephthalate

Refernces