Technology Process of 3-amino-2-benzoyl-1H-inden-1-one
There total 8 articles about 3-amino-2-benzoyl-1H-inden-1-one which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
bis-triphenylphosphine-palladium(II) chloride; carbon monoxide; triethylamine;
In
dichloromethane;
at 100 ℃;
for 4h;
under 15201 Torr;
DOI:10.1021/acs.joc.0c01282
- Guidance literature:
-
With
bis-triphenylphosphine-palladium(II) chloride; triethylamine;
In
dichloromethane;
at 100 ℃;
for 4h;
under 15201 Torr;
Temperature;
Catalytic behavior;
Inert atmosphere;
Schlenk technique;
Autoclave;
DOI:10.1021/acs.joc.0c01282
- Guidance literature:
-
Multi-step reaction with 4 steps
1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / N,N-dimethyl-formamide / 24 h / Reflux
2: cesium fluoride / methanol / 3 h / 20 °C
3: bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 4 h / 100 °C / 15201 Torr / Inert atmosphere; Schlenk technique; Autoclave
4: bis-triphenylphosphine-palladium(II) chloride; triethylamine; carbon monoxide / dichloromethane / 4 h / 100 °C / 15201 Torr
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; carbon monoxide; triethylamine; cesium fluoride;
In
methanol; dichloromethane; N,N-dimethyl-formamide;
3: |Sonogashira Cross-Coupling / 4: |Sonogashira Cross-Coupling;
DOI:10.1021/acs.joc.0c01282
