Technology Process of C31H18F6N4O2
There total 6 articles about C31H18F6N4O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium phosphate;
palladium diacetate; triphenylphosphine;
In
N,N-dimethyl-formamide;
at 110 ℃;
for 0.333333h;
Inert atmosphere;
Microwave irradiation;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium carbonate / dimethyl sulfoxide / 2 h / 40 °C
2: sodium tetrahydroborate / ethanol / 0 °C
3: iodine; sodium carbonate / methanol / 20 °C
4: thionyl chloride / chloroform / 20 - 40 °C
5: potassium phosphate / palladium diacetate; triphenylphosphine / N,N-dimethyl-formamide / 0.33 h / 110 °C / Inert atmosphere; Microwave irradiation
With
sodium tetrahydroborate; potassium phosphate; thionyl chloride; iodine; sodium carbonate; potassium carbonate;
palladium diacetate; triphenylphosphine;
In
methanol; ethanol; chloroform; dimethyl sulfoxide; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium tetrahydroborate / ethanol / 0 °C
2: iodine; sodium carbonate / methanol / 20 °C
3: thionyl chloride / chloroform / 20 - 40 °C
4: potassium phosphate / palladium diacetate; triphenylphosphine / N,N-dimethyl-formamide / 0.33 h / 110 °C / Inert atmosphere; Microwave irradiation
With
sodium tetrahydroborate; potassium phosphate; thionyl chloride; iodine; sodium carbonate;
palladium diacetate; triphenylphosphine;
In
methanol; ethanol; chloroform; N,N-dimethyl-formamide;
