O,O-Diphenyl-N-chlorophosphoramidat

Base Information

• Chemical Name: O,O-Diphenyl-N-chlorophosphoramidat
• CAS No.: 75119-98-1
• Molecular Formula: C₁₂H₁₁ClNO₃P
• Molecular Weight: 283.651
• Mol file: 75119-98-1.mol

Synonyms:O,O-Diphenyl-N-chlorophosphoramidat

Chemical Property of O,O-Diphenyl-N-chlorophosphoramidat

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of O,O-Diphenyl-N-chlorophosphoramidat

There total 3 articles about O,O-Diphenyl-N-chlorophosphoramidat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

dichloro-phosphoramidic acid diphenyl ester (27125-51-5) → O,O-Diphenyl-N-chlorophosphoramidat (75119-98-1)

Guidance literature:

With water; In Petroleum ether; at 55 - 60 ℃;

Reference yield: 78.6%

diphenylphosphoroamidate (2015-56-7) → O,O-Diphenyl-N-chlorophosphoramidat (75119-98-1)

Guidance literature:

With tert-butylhypochlorite; In methanol;

Reference yield:

diphenylphosphoroamidate (2015-56-7) + dichloro-phosphoramidic acid diphenyl ester (27125-51-5) → O,O-Diphenyl-N-chlorophosphoramidat (75119-98-1)

Guidance literature:

Heating;

upstream raw materials:

diphenylphosphoroamidate

dichloro-phosphoramidic acid diphenyl ester

Downstream raw materials:

C₃₀H₂₅N₃O₈P₂S

C₃₀H₂₅ClN₂O₆P₂S

C₃₀H₂₅N₃O₈P₂S

C₃₁H₂₈N₂O₆P₂S

Refernces

• 1、 Kharchenko, A. V.,Koval, I. V.,Kremlev, M. M.. "IMINATION OF SULFUR-CONTAINING COMPOUNDS. XIII. DIPHENOXYPHOSPHINOYLIMINATION OF THIOLS AND DISULFIDES". . p. 662 - 665. Retrieved 2007/10/02.