triphenylmethyl 4-cyanophenyl ether

Base Information

• Chemical Name: triphenylmethyl 4-cyanophenyl ether
• CAS No.: 95953-45-0
• Molecular Formula: C₂₆H₁₉NO
• Molecular Weight: 361.443
• Mol file: 95953-45-0.mol

Synonyms:triphenylmethyl 4-cyanophenyl ether

Chemical Property of triphenylmethyl 4-cyanophenyl ether

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of triphenylmethyl 4-cyanophenyl ether

There total 3 articles about triphenylmethyl 4-cyanophenyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-cyanophenol (767-00-0) + trityl chloride (76-83-5) → triphenylmethyl 4-cyanophenyl ether (95953-45-0)

Guidance literature:

With potassium hydride; Multistep reaction; 1.) THF, 1 h, 2.) reflux;

DOI:10.1021/ja00193a031

Reference yield:

bromo-triphenyl-methane (596-43-0) + silver tetrakis-(4-cyanophenyl)aluminate (1449788-41-3) → triphenylmethyl 4-cyanophenyl ether (95953-45-0)

Guidance literature:

In acetonitrile; at 20 ℃; Darkness;

DOI:10.1002/zaac.201300030

Reference yield:

→ triphenylmethyl 4-cyanophenyl ether (95953-45-0)

Guidance literature:

Na-<4-cyan-phenolat>, Triphenylmethylchlorid, sd. Bzl., 3h;

DOI:10.1021/ja00890a020

upstream raw materials:

4-cyanophenol

trityl chloride

bromo-triphenyl-methane

silver tetrakis-(4-cyanophenyl)aluminate

Downstream raw materials:

2,2,2-triphenylacetonitrile

2,2,2-trifluoroethyl-O-trityl eher

propyl-trityl-amine

N-tritylimidazole

Refernces

• 1、 McClelland, Robert A.,Kanagasabapathy, V. M.,Banait, Narinder S.,Steenken, Steen. "Flash-Photolysis Generation and Reactivities of Triarylmethyl and Diarylmethyl Cations in Aqueous Solutions". . p. 3966 - 3972. Retrieved 2007/10/02.