C₂₉H₄₄N₄O₇

Base Information

• Chemical Name: C₂₉H₄₄N₄O₇
• CAS No.: 934400-61-0
• Molecular Formula: C₂₉H₄₄N₄O₇
• Molecular Weight: 560.691
• Mol file: 934400-61-0.mol

Synonyms:C₂₉H₄₄N₄O₇

Chemical Property of C₂₉H₄₄N₄O₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₉H₄₄N₄O₇

There total 17 articles about C₂₉H₄₄N₄O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C30H40O5SSi → C29H44N4O7 (934400-61-0)

Guidance literature:

Multi-step reaction with 10 steps

1.1: 0.929 g / NaN₃ / dimethylformamide / 5 h / 60 °C

2.1: H₂ / PtO₂ / ethyl acetate

3.1: 1.96 g / triethylamine / CH₂Cl₂ / 20 °C

4.1: 97 percent / H₂ / Pd/C / ethanol

5.1: 82 percent / oxalyl chloride; methyl sulfoxide; Et₃N / CH₂Cl₂ / -78 - 20 °C

6.1: potassium 1,1,1,3,3,3-hexamethyldisilylamide / tetrahydrofuran / 1 h / -78 °C

6.2: 94 percent / tetrahydrofuran / -78 - 20 °C

7.1: 82 percent / pyridine; HF / 3 h / 0 °C

8.1: 72 percent / 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; NaClO₂; NaClO / acetonitrile; aq. phosphate buffer / 35 °C / pH 6.85

9.1: diisopropylethylamine; 1-hydroxybenzotriazole; N-(3-dimethylaminopropyl)-N'-ethylcarbodiimide / CH₂Cl₂ / 0.33 h / 0 °C

9.2: 72 percent / CH₂Cl₂ / 16 h / 0 - 20 °C

10.1: trifluoroacetic acid / CH₂Cl₂ / 5 h

With pyridine; 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; sodium chlorite; sodium azide; oxalyl dichloride; free radical; hydrogen fluoride; hydrogen; benzotriazol-1-ol; dimethyl sulfoxide; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; platinum(IV) oxide; palladium on activated charcoal; In tetrahydrofuran; phosphate buffer; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetonitrile; 5.1: Swern oxidation;

DOI:10.1021/ja0686256

Reference yield:

C14H20O2 → C29H44N4O7 (934400-61-0)

Guidance literature:

Multi-step reaction with 14 steps

1.1: 0.543 g / pyridine / CH₂Cl₂

2.1: 93 percent / 4-dimethylaminopyridine / pyridine / CH₂Cl₂ / 0 - 20 °C

3.1: triethylamine / tetrahydrofuran / 20 °C

4.1: 0.929 g / NaN₃ / dimethylformamide / 5 h / 60 °C

5.1: H₂ / PtO₂ / ethyl acetate

6.1: 1.96 g / triethylamine / CH₂Cl₂ / 20 °C

7.1: 97 percent / H₂ / Pd/C / ethanol

8.1: 82 percent / oxalyl chloride; methyl sulfoxide; Et₃N / CH₂Cl₂ / -78 - 20 °C

9.1: potassium 1,1,1,3,3,3-hexamethyldisilylamide / tetrahydrofuran / 1 h / -78 °C

9.2: 94 percent / tetrahydrofuran / -78 - 20 °C

10.1: 82 percent / pyridine; HF / 3 h / 0 °C

11.1: 72 percent / 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; NaClO₂; NaClO / acetonitrile; aq. phosphate buffer / 35 °C / pH 6.85

12.1: diisopropylethylamine; 1-hydroxybenzotriazole; N-(3-dimethylaminopropyl)-N'-ethylcarbodiimide / CH₂Cl₂ / 0.33 h / 0 °C

12.2: 72 percent / CH₂Cl₂ / 16 h / 0 - 20 °C

13.1: trifluoroacetic acid / CH₂Cl₂ / 5 h

With pyridine; dmap; 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; sodium chlorite; sodium azide; oxalyl dichloride; free radical; hydrogen fluoride; hydrogen; benzotriazol-1-ol; dimethyl sulfoxide; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; pyridine; platinum(IV) oxide; palladium on activated charcoal; In tetrahydrofuran; phosphate buffer; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetonitrile; 9.1: Swern oxidation;

DOI:10.1021/ja0686256

Reference yield:

C29H39NO2Si → C29H44N4O7 (934400-61-0)

Guidance literature:

Multi-step reaction with 8 steps

1.1: 1.96 g / triethylamine / CH₂Cl₂ / 20 °C

2.1: 97 percent / H₂ / Pd/C / ethanol

3.1: 82 percent / oxalyl chloride; methyl sulfoxide; Et₃N / CH₂Cl₂ / -78 - 20 °C

4.1: potassium 1,1,1,3,3,3-hexamethyldisilylamide / tetrahydrofuran / 1 h / -78 °C

4.2: 94 percent / tetrahydrofuran / -78 - 20 °C

5.1: 82 percent / pyridine; HF / 3 h / 0 °C

6.1: 72 percent / 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; NaClO₂; NaClO / acetonitrile; aq. phosphate buffer / 35 °C / pH 6.85

7.1: diisopropylethylamine; 1-hydroxybenzotriazole; N-(3-dimethylaminopropyl)-N'-ethylcarbodiimide / CH₂Cl₂ / 0.33 h / 0 °C

7.2: 72 percent / CH₂Cl₂ / 16 h / 0 - 20 °C

8.1: trifluoroacetic acid / CH₂Cl₂ / 5 h

With pyridine; 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; sodium chlorite; oxalyl dichloride; free radical; hydrogen fluoride; hydrogen; benzotriazol-1-ol; dimethyl sulfoxide; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; phosphate buffer; ethanol; dichloromethane; acetonitrile; 3.1: Swern oxidation;

DOI:10.1021/ja0686256

upstream raw materials:

C₃₈H₆₀N₄O₉

C₂₇H₄₁NO₄Si

C₂₇H₃₉NO₄Si

C₃₃H₄₉NO₅Si

Downstream raw materials:

C₂₉H₄₂N₄O₆

Refernces