Technology Process of 6-ethoxycarbonyl-2-phenylindole
There total 5 articles about 6-ethoxycarbonyl-2-phenylindole which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dihydridotetrakis(triphenylphosphine)ruthenium; allyl methyl carbonate;
In
toluene;
at 100 ℃;
for 24h;
DOI:10.1002/jhet.5570290509
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 84 percent / sodium ethoxide / dimethylsulfoxide / 24 h / Ambient temperature
2: 88 percent / iron powder, conc. hydrochloric acid / methanol; H2O / 24 h / Heating
3: 82 percent / allyl methyl carbonate, dihydridotetrikis(triphenylphosphine)ruthenium(II) / toluene / 24 h / 100 °C
With
hydrogenchloride; dihydridotetrakis(triphenylphosphine)ruthenium; allyl methyl carbonate; sodium ethanolate; iron;
In
methanol; water; dimethyl sulfoxide; toluene;
DOI:10.1002/jhet.5570290509
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 84 percent / sodium ethoxide / dimethylsulfoxide / 24 h / Ambient temperature
2: 88 percent / iron powder, conc. hydrochloric acid / methanol; H2O / 24 h / Heating
3: 82 percent / allyl methyl carbonate, dihydridotetrikis(triphenylphosphine)ruthenium(II) / toluene / 24 h / 100 °C
With
hydrogenchloride; dihydridotetrakis(triphenylphosphine)ruthenium; allyl methyl carbonate; sodium ethanolate; iron;
In
methanol; water; dimethyl sulfoxide; toluene;
DOI:10.1002/jhet.5570290509