Phosphenimidous amide,N,N'-diphenyl-

Base Information

• Chemical Name: Phosphenimidous amide,N,N'-diphenyl-
• CAS No.: 5679-59-4
• Molecular Formula: C12H11 N2 P
• Molecular Weight: 214.207
• Mol file: 5679-59-4.mol

Synonyms:Phosphine,anilino(phenylimino)- (5CI); NSC 5726

Chemical Property of Phosphenimidous amide,N,N'-diphenyl-

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: g/cm³

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Phosphenimidous amide,N,N'-diphenyl-

There total 2 articles about Phosphenimidous amide,N,N'-diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

aniline (62-53-3) → diphenylphosphazoanilide (5679-59-4)

Guidance literature:

With phosphorus trichloride; In toluene; for 2h; Heating;

DOI:10.1016/S0040-4039(00)88859-0

Reference yield:

→ diphenylphosphazoanilide (5679-59-4)

Guidance literature:

Anilin, PCl3;

DOI:10.1039/jr9600003371

Reference yield: 87.0%

diphenylphosphazoanilide (5679-59-4) + (E)-but-2-enoic acid (107-93-7) → (E)-crotonanilide (17645-30-6)

Guidance literature:

In tetrahydrofuran; for 18h; Heating;

DOI:10.1016/S0040-4039(00)88859-0

upstream raw materials:

aniline

Downstream raw materials:

N-phenyl-2-hydroxy-3-methyl-butanamide

(E)-crotonanilide

N-acryloylaniline

3-benzyl-4-phenyl-5-(2-(phenylselanyl)ethyl)-4H-[1,2,4]triazole

Refernces

• 1、 Amir, Mohammad,Ali, Israr. "Novel approach for the synthesis of N-substituted-4-(2-methyl-4-oxo- 4hquinazolin- 3-YL)-butyramides". experimental part. p. 2086 - 2095. Retrieved 2011/07/31.
• 2、 Cabral, Jose,Laszlo, Pierre,Montaufier, Marie-Therese,Lalatiana Randriamahefa. "The phosphazo route to 2-alkenamides from acrylic acid and its derivatives". . p. 1705 - 1708. Retrieved 2007/10/02.