2-bromo-6-fluorobenzaldehyde hydrazone

Base Information

• Chemical Name: 2-bromo-6-fluorobenzaldehyde hydrazone
• CAS No.: 914311-44-7
• Molecular Formula: C₇H₆BrFN₂
• Molecular Weight: 217.04
• Mol file: 914311-44-7.mol

Synonyms:2-bromo-6-fluorobenzaldehyde hydrazone

Chemical Property of 2-bromo-6-fluorobenzaldehyde hydrazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 2-bromo-6-fluorobenzaldehyde hydrazone

There total 1 articles about 2-bromo-6-fluorobenzaldehyde hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

2-bromo-6-fluorobenzaldehyde (360575-28-6) → 2-bromo-6-fluorobenzaldehyde hydrazone (914311-44-7)

Guidance literature:

With hydrazine hydrate; In water; toluene; at 50 ℃; for 1.5h;

DOI:10.1021/jo0613784

Reference yield: 100.0%

2-bromo-6-fluorobenzaldehyde hydrazone (914311-44-7) → 1-bromo-3-fluoro-2-methyl-benzene (1422-54-4)

Guidance literature:

With sodium hydrogencarbonate;

DOI:10.1021/jo0613784

Reference yield:

2-bromo-6-fluorobenzaldehyde hydrazone (914311-44-7) → 1-bromo-3-fluoro-2-methyl-benzene (1422-54-4) + 4-bromoindazole (186407-74-9)

Guidance literature:

With potassium carbonate; hydrazine hydrate; at 90 - 100 ℃; for 5h;

DOI:10.1021/jo0613784

upstream raw materials:

2-bromo-6-fluorobenzaldehyde

Downstream raw materials:

1-bromo-3-fluoro-2-methyl-benzene

4-bromoindazole

2-benzyl-4-bromo-2H-indazole

1-benzyl-4-bromoindazole

Refernces