3-Hydroxy-1-indenone

Base Information

• Chemical Name: 3-Hydroxy-1-indenone
• CAS No.: 70432-32-5
• Molecular Formula: C₉H₆O₂
• Molecular Weight: 146.145
• Mol file: 70432-32-5.mol

Synonyms:3-Hydroxy-1-indenone

Chemical Property of 3-Hydroxy-1-indenone

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 3-Hydroxy-1-indenone

There total 1 articles about 3-Hydroxy-1-indenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

Ethyl (Z)-3-(4-acetylphenylthio)cinnamate (128671-32-9) → 4-mercaptoacetophenone (3814-20-8) + 3-Hydroxy-1-indenone (70432-32-5) + ethyl 3-oxo-3-phenylpropionate (94-02-0)

Guidance literature:

With sulfuric acid; at 20 ℃; for 1h;

DOI:10.1246/bcsj.63.847

Reference yield: 95.0%

tributylphosphine (998-40-3) + C26H39O5P (1369321-88-9) + 3-Hydroxy-1-indenone (70432-32-5) → C47H70O6P2 (1369322-06-4)

Guidance literature:

With pyrrolidine; benzoic acid; In tetrahydrofuran; at 28 - 30 ℃; for 0.5h; chemoselective reaction; Inert atmosphere;

DOI:10.1021/ol3005479

Reference yield: 90.0%

tributylphosphine (998-40-3) + 3-Hydroxy-1-indenone (70432-32-5) + terephthalaldehyde, (623-27-8) → C29H37O3P (1369321-87-8)

Guidance literature:

With pyrrolidine; benzoic acid; In tetrahydrofuran; at 28 - 30 ℃; for 0.5h; chemoselective reaction; Inert atmosphere;

DOI:10.1021/ol3005479

upstream raw materials:

Ethyl (Z)-3-(4-acetylphenylthio)cinnamate

Downstream raw materials:

C₄₇H₇₀O₆P₂

C₂₉H₃₇O₃P

C₂₈H₃₇O₂P

Refernces