methyl (2S)-2-amino-3-cyclohexa-1,4-dien-1-ylpropanoate hydrochloride

Base Information

• Chemical Name: methyl (2S)-2-amino-3-cyclohexa-1,4-dien-1-ylpropanoate hydrochloride
• CAS No.: 33423-61-9
• Molecular Formula: C₁₀H₁₅NO₂*ClH
• Molecular Weight: 217.696
• Mol file: 33423-61-9.mol

Synonyms:methyl (2S)-2-amino-3-cyclohexa-1,4-dien-1-ylpropanoate hydrochloride

Chemical Property of methyl (2S)-2-amino-3-cyclohexa-1,4-dien-1-ylpropanoate hydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of methyl (2S)-2-amino-3-cyclohexa-1,4-dien-1-ylpropanoate hydrochloride

There total 1 articles about methyl (2S)-2-amino-3-cyclohexa-1,4-dien-1-ylpropanoate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(L)-(-)-2,5-dihydro-phenylalanine (16055-12-2,29821-30-5) → methyl (2S)-2-amino-3-cyclohexa-1,4-dien-1-ylpropanoate hydrochloride (33423-61-9)

Guidance literature:

With thionyl chloride; In methanol;

Reference yield: 93.0%

methyl (2S)-2-amino-3-cyclohexa-1,4-dien-1-ylpropanoate hydrochloride (33423-61-9) + 5-chloro-5H-dibenzo[a,d]cycloheptene (18506-04-2) → methyl (2S)-3-(cyclohexa-1,4-dienyl)-2-(5H-dibenzo[a,d]cyclohepten-5-yl-amino)propionate

Guidance literature:

methyl (2S)-2-amino-3-cyclohexa-1,4-dien-1-ylpropanoate hydrochloride; With triethylamine; In dichloromethane; for 0.5h;

5-chloro-5H-dibenzo[a,d]cycloheptene; In dichloromethane; for 2h;

DOI:10.1002/ejic.200900875

upstream raw materials:

(L)-(-)-2,5-dihydro-phenylalanine

Refernces