C₆₄H₅₈O₁₂S

Base Information

• Chemical Name: C₆₄H₅₈O₁₂S
• CAS No.: 148014-76-0
• Molecular Formula: C₆₄H₅₈O₁₂S
• Molecular Weight: 1051.22
• Mol file: 148014-76-0.mol

Synonyms:C₆₄H₅₈O₁₂S

Chemical Property of C₆₄H₅₈O₁₂S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₄H₅₈O₁₂S

There total 10 articles about C₆₄H₅₈O₁₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Benzyloxy-2-methoxy-3,5,6-trimethyl-benzoyl chloride (148014-36-2) → C64H58O12S (148014-76-0)

Guidance literature:

Multi-step reaction with 4 steps

1: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 30 min, 2.) THF, hexane, from -78 deg C, 10 min to RT, overnight

2: H₂ / Pd/C / methanol; ethyl acetate

3: ethyl acetate / Ambient temperature

4: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 30 min, 2.) THF, hexane, from -78 deg C, 10 min to RT, overnight

With n-butyllithium; hydrogen; palladium on activated charcoal; In methanol; ethyl acetate;

DOI:10.1021/jm960437a

Reference yield:

4-Benzyloxy-2-methoxy-3,5,6-trimethyl-benzoic acid → C64H58O12S (148014-76-0)

Guidance literature:

Multi-step reaction with 5 steps

1: oxalyl chloride / CH₂Cl₂ / a) RT, 30 min, b) reflux, 30 min

2: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 30 min, 2.) THF, hexane, from -78 deg C, 10 min to RT, overnight

3: H₂ / Pd/C / methanol; ethyl acetate

4: ethyl acetate / Ambient temperature

5: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 30 min, 2.) THF, hexane, from -78 deg C, 10 min to RT, overnight

With n-butyllithium; oxalyl dichloride; hydrogen; palladium on activated charcoal; In methanol; dichloromethane; ethyl acetate;

DOI:10.1021/jm960437a

Reference yield:

C42H42O7 (148014-38-4) → C64H58O12S (148014-76-0)

Guidance literature:

Multi-step reaction with 3 steps

1: H₂ / Pd/C / methanol; ethyl acetate

2: ethyl acetate / Ambient temperature

3: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 30 min, 2.) THF, hexane, from -78 deg C, 10 min to RT, overnight

With n-butyllithium; hydrogen; palladium on activated charcoal; In methanol; ethyl acetate;

DOI:10.1021/jm960437a

upstream raw materials:

5-(3-Chlorocarbonyl-4-methoxy-phenylsulfanyl)-2-methoxy-benzoic acid benzhydryl ester

benzhydryl 4-(2-methoxy-3,5,6-trimethyl-4-hydroxybenzoyloxy)-2-methoxy-3,5,6-trimethylbenzoate

5,5'-thio-bis(2-hydroxy-benzoic acid)

6,6'-dimethoxy-3,3'-sulfanediyl-di-benzoic acid

Refernces