C₁₉H₁₆BrN

Base Information

• Chemical Name: C₁₉H₁₆BrN
• CAS No.: 717880-57-4
• Molecular Formula: C₁₉H₁₆BrN
• Molecular Weight: 338.247
• Mol file: 717880-57-4.mol

Synonyms:C₁₉H₁₆BrN

Chemical Property of C₁₉H₁₆BrN

Chemical Property:

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₉H₁₆BrN

There total 2 articles about C₁₉H₁₆BrN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

N,N-diphenyl-m-toluidine (4316-54-5) → C19H16BrN (717880-57-4)

Guidance literature:

With Oxone; copper(ll) bromide; In acetonitrile; at 20 ℃; for 3h; regioselective reaction;

DOI:10.1039/c3ra41664j

Reference yield: 25.0%

→ C19H16BrN (717880-57-4)

Guidance literature:

With 1,10-Phenanthroline; copper(l) chloride; potassium hydroxide; In toluene; at 120 ℃; for 24h; Inert atmosphere;

upstream raw materials:

N,N-diphenyl-m-toluidine

Refernces

• 1、 Li, Xin-Le,Wu, Wei,Fan, Xin-Heng,Yang, Lian-Ming. "A facile, regioselective and controllable bromination of aromatic amines using a CuBr2/Oxone system". . p. 12091 - 12095. Retrieved 2013/09/02.