[HC[(CMe)(N-2,6-iPr2C6H3)2]2]2 (μ-oxo)dialuminum dihydroxide

Base Information Edit

Chemical Name:[HC[(CMe)(N-2,6-iPr2C6H3)2]2]2 (μ-oxo)dialuminum dihydroxide
CAS No.:647841-64-3
Molecular Formula:C₅₈H₈₄Al₂N₄O₃
Molecular Weight:939.293
Hs Code.:
Mol file:647841-64-3.mol

Synonyms:[HC[(CMe)(N-2,6-iPr2C6H3)2]2]2 (μ-oxo)dialuminum dihydroxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [HC[(CMe)(N-2,6-iPr2C6H3)2]2]2 (μ-oxo)dialuminum dihydroxide Edit

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Technology Process of [HC[(CMe)(N-2,6-iPr2C6H3)2]2]2 (μ-oxo)dialuminum dihydroxide

There total 2 articles about [HC[(CMe)(N-2,6-iPr2C6H3)2]2]2 (μ-oxo)dialuminum dihydroxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 325465-26-7
Dipp₂nacnacAlI₂

: 7664-41-7
ammonia

: 7732-18-5
water

: 865-37-2
dimethylaluminum hydride

: potassium hydroxide

: 647841-64-3
[HC[(CMe)(N-2,6-iPr2C6H3)2]2]2 (μ-oxo)dialuminum dihydroxide

Guidance literature:: With KH; In toluene; NH3 condensed onto suspn. of Al-complex, KOH, H2O and KH in toluene at -78 °C under stirring, mixt. stirred for 1 h; NH3 evapd. over 4 h while mixt. heated to room temp., mixt. filtered, concd. (vac.), hexane added, soln. kept at -20 °C for 2 d.; elem. anal.;