C₁₅H₁₅NO₄S

Base Information

• Chemical Name: C₁₅H₁₅NO₄S
• CAS No.: 927197-16-8
• Molecular Formula: C₁₅H₁₅NO₄S
• Molecular Weight: 305.354
• Mol file: 927197-16-8.mol

Synonyms:C₁₅H₁₅NO₄S

Chemical Property of C₁₅H₁₅NO₄S

Chemical Property:

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Technology Process of C₁₅H₁₅NO₄S

There total 1 articles about C₁₅H₁₅NO₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

thiophene-2,5-dicarboxylic acid monomethyl ester (50340-79-9) + 2-methyl-4-methoxyaniline (102-50-1) → C15H15NO4S (927197-16-8)

Guidance literature:

thiophene-2,5-dicarboxylic acid monomethyl ester; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 0.166667h;

2-methyl-4-methoxyaniline; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield: 90.0%

C15H15NO4S (927197-16-8) → C14H13NO4S (927197-17-9)

Guidance literature:

C₁₅H₁₅NO₄S; With methanol; lithium hydroxide; water; In tetrahydrofuran; at 20 ℃; for 3h;

With hydrogenchloride; In water; pH=~ 3;

Reference yield: 68.0%

C15H15NO4S (927197-16-8) + methyl iodide (74-88-4) → C16H17NO4S

Guidance literature:

C₁₅H₁₅NO₄S; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.166667h;

methyl iodide; In N,N-dimethyl-formamide; at 40 ℃;

upstream raw materials:

thiophene-2,5-dicarboxylic acid monomethyl ester

2-methyl-4-methoxyaniline

Downstream raw materials:

C₁₄H₁₃NO₄S

Refernces