Technology Process of C52H90S2
There total 4 articles about C52H90S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 69 percent / CuBr*Me2S / diethyl ether; cyclohexane / 24 h / Ambient temperature
2: 73 percent / ClSO3H / CHCl3 / 22 h / Ambient temperature
3: 1.) P, I2, AcOH, 2.) H2O / 1.) reflux, 23 h, 2.) reflux, 1 h
With
chlorosulfonic acid; copper(I) bromide dimethylsulfide complex; water; iodine; acetic acid;
In
diethyl ether; chloroform; cyclohexane;
DOI:10.1055/s-1999-3498
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 73 percent / ClSO3H / CHCl3 / 22 h / Ambient temperature
2: 1.) P, I2, AcOH, 2.) H2O / 1.) reflux, 23 h, 2.) reflux, 1 h
With
chlorosulfonic acid; water; iodine; acetic acid;
In
chloroform;
DOI:10.1055/s-1999-3498
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 69 percent / CuBr*Me2S / diethyl ether; cyclohexane / 24 h / Ambient temperature
2: 73 percent / ClSO3H / CHCl3 / 22 h / Ambient temperature
3: 1.) P, I2, AcOH, 2.) H2O / 1.) reflux, 23 h, 2.) reflux, 1 h
With
chlorosulfonic acid; copper(I) bromide dimethylsulfide complex; water; iodine; acetic acid;
In
diethyl ether; chloroform; cyclohexane;
DOI:10.1055/s-1999-3498