Technology Process of C51H33N5
There total 5 articles about C51H33N5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate;
In
5,5-dimethyl-1,3-cyclohexadiene;
for 8h;
Inert atmosphere;
Reflux;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / toluene; water / 8 h / 80 °C / Inert atmosphere
2: triphenylphosphine / 1,2-dichloro-benzene / 8 h / 180 °C / Inert atmosphere
3: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / toluene; water; 1,2-dimethoxyethane / 8 h / 80 °C / Inert atmosphere
4: tris-(dibenzylideneacetone)dipalladium(0); tri tert-butylphosphoniumtetrafluoroborate; sodium t-butanolate / 5,5-dimethyl-1,3-cyclohexadiene / 8 h / Inert atmosphere; Reflux
With
tris-(dibenzylideneacetone)dipalladium(0); tetrakis(triphenylphosphine) palladium(0); sodium carbonate; triphenylphosphine; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate;
In
1,2-dimethoxyethane; 5,5-dimethyl-1,3-cyclohexadiene; water; 1,2-dichloro-benzene; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / toluene; water / 8 h / 80 °C / Inert atmosphere
2: triphenylphosphine / 1,2-dichloro-benzene / 8 h / 180 °C / Inert atmosphere
3: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / toluene; water; 1,2-dimethoxyethane / 8 h / 80 °C / Inert atmosphere
4: tris-(dibenzylideneacetone)dipalladium(0); tri tert-butylphosphoniumtetrafluoroborate; sodium t-butanolate / 5,5-dimethyl-1,3-cyclohexadiene / 8 h / Inert atmosphere; Reflux
With
tris-(dibenzylideneacetone)dipalladium(0); tetrakis(triphenylphosphine) palladium(0); sodium carbonate; triphenylphosphine; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate;
In
1,2-dimethoxyethane; 5,5-dimethyl-1,3-cyclohexadiene; water; 1,2-dichloro-benzene; toluene;