dihydrooxyresveratrol

Base Information

• Chemical Name: dihydrooxyresveratrol
• CAS No.: 24082-42-6
• Molecular Formula: C₁₄H₁₄O₄
• Molecular Weight: 246.263
• Mol file: 24082-42-6.mol

Synonyms:dihydrooxyresveratrol

Chemical Property of dihydrooxyresveratrol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of dihydrooxyresveratrol

There total 11 articles about dihydrooxyresveratrol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.6%

oxyresveratrol (4721-07-7,29700-22-9) → dihydrooxyresveratrol (24082-42-6)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; at 20 ℃; for 1h; under 35252.8 Torr;

DOI:10.1016/j.bmcl.2006.08.018

Reference yield: 76.0%

2,4-di(tert-butyldiphenylsilyloxy)-3′,5′-dihydroxybibenzyl → dihydrooxyresveratrol (24082-42-6)

Guidance literature:

With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; acetonitrile; at 20 ℃; for 0.5h;

DOI:10.1016/j.carres.2018.11.006

Reference yield:

oxyresveratrol (4721-07-7,29700-22-9) + ethyl acetoacetate (141-97-9) → dihydrooxyresveratrol (24082-42-6)

Guidance literature:

With hydrogen; palladium on activated charcoal;

DOI:10.1002/ardp.19813141205

upstream raw materials:

oxyresveratrol

ethyl acetoacetate

2-(3,5-dihydroxyphenyl)acetic acid

2,4-Dihydroxybenzaldehyde

Downstream raw materials:

2,4,3',5'-tetramethoxy-bibenzyl

Ethandiyl-1-(3-benzyl-8-methoxy-5,5-dimethyl-1,2,3,4-tetrahydro-5H-benzopyrano-<3,4-c>-9-pyridin)-2-(3-benzyl-10-methoxy-5,5-dimethyl-1,2,3,4-tetrahydro-5H-benzopyrano-<3,4-c>-8-pyridin)

Ethandiyl-1-(3-benzyl-8-hydroxy-5-oxo-1,2,3,4-tetrahydro-5H-benzopyrano-<3,4-c>-9-pyridin)-2-(3-benzyl-10-hydroxy-5-oxo-1,2,3,4-tetrahydro-5H-benzopyrano-<3,4-c>-8-pyridin)

2,4,3',5'-tetraacetoxy-bibenzyl

Refernces

• 1、 -. "Synthetic method for natural product 2,3',4,5'-tetrahydroxy bibenzyl". Paragraph 0021; 0033-0034; 0041; 0048; 0055; 0062; 0069. . Retrieved 2017/08/28.
• 2、 Likhitwitayawuid, Kittisak,Sornsute, Acom,Sritularak, Boonchoo,Ploypradith, Poonsakdi. "Chemical transformations of oxyresveratrol (trans-2,4,3′,5′-tetrahydroxystilbene) into a potent tyrosinase inhibitor and a strong cytotoxic agent". . p. 5650 - 5653. Retrieved 2007/10/03.