C₂₄H₂₃NS

Base Information

• Chemical Name: C₂₄H₂₃NS
• CAS No.: 86864-33-7
• Molecular Formula: C₂₄H₂₃NS
• Molecular Weight: 357.519
• Mol file: 86864-33-7.mol

Synonyms:C₂₄H₂₃NS

Chemical Property of C₂₄H₂₃NS

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₂₄H₂₃NS

There total 3 articles about C₂₄H₂₃NS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

3,3-dimethyl acrylaldehyde (107-86-8) + Triphenylmethanesulfenamide (38499-08-0) → C24H23NS (86864-33-7)

Guidance literature:

With pyridinium p-toluenesulfonate; magnesium sulfate; In dichloromethane; for 2h; Ambient temperature;

DOI:10.1021/jo00168a031

Reference yield:

triphenylmethanethiol (3695-77-0) → C24H23NS (86864-33-7)

Guidance literature:

Multi-step reaction with 3 steps

1: 88 percent / Sulfuryl chloride / toluene; diethyl ether / 2 h / 0 °C

2: 78 percent / 29 percent NH₄OH/H₂O / CH₂Cl₂ / 0 °C

3: 92 percent / Pyridinium p-toluenesulfonate, (PPTS)/anhydr. MgSO₄ / CH₂Cl₂ / 2 h / Ambient temperature

With ammonium hydroxide; sulfuryl dichloride; water; pyridinium p-toluenesulfonate; magnesium sulfate; In diethyl ether; dichloromethane; toluene;

DOI:10.1021/jo00168a031

Reference yield:

tritylsulfenyl chloride (24165-03-5) → C24H23NS (86864-33-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 78 percent / 29 percent NH₄OH/H₂O / CH₂Cl₂ / 0 °C

2: 92 percent / Pyridinium p-toluenesulfonate, (PPTS)/anhydr. MgSO₄ / CH₂Cl₂ / 2 h / Ambient temperature

With ammonium hydroxide; water; pyridinium p-toluenesulfonate; magnesium sulfate; In dichloromethane;

DOI:10.1021/jo00168a031

upstream raw materials:

3,3-dimethyl acrylaldehyde

Triphenylmethanesulfenamide

triphenylmethanethiol

tritylsulfenyl chloride

Refernces