dihydro-β-damascol

Base Information

• Chemical Name: dihydro-β-damascol
• CAS No.: 42742-79-0
• Molecular Formula: C₁₃H₂₄O
• Molecular Weight: 196.333
• Mol file: 42742-79-0.mol

Synonyms:dihydro-β-damascol

Chemical Property of dihydro-β-damascol

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of dihydro-β-damascol

There total 3 articles about dihydro-β-damascol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

1-(2,6,6-trimethylcyclohex-1-en-1-yl)butan-1-one (28384-26-1) → dihydro-β-damascol (42742-79-0)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; for 5h;

DOI:10.1039/c4ra03939d

Reference yield:

1-(2,2,6-trimethylcyclohex-1-ene-yl)but-3-en-1-ol (28897-21-4) → dihydro-β-damascol (42742-79-0)

Guidance literature:

With hydrogen; nickel; In ethanol;

DOI:10.1002/hlca.19710540718

Reference yield:

beta damascone (23726-91-2) → dihydro-β-damascol (42742-79-0)

Guidance literature:

Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / diethyl ether / 5 h

2: lithium aluminium tetrahydride / diethyl ether / 5 h

With lithium aluminium tetrahydride; In diethyl ether;

DOI:10.1039/c4ra03939d

upstream raw materials:

1-(2,2,6-trimethylcyclohex-1-ene-yl)but-3-en-1-ol

beta damascone

1-(2,6,6-trimethylcyclohex-1-en-1-yl)butan-1-one

Downstream raw materials:

Acetic acid 1-(2,6,6-trimethyl-cyclohex-1-enyloxy)-butyl ester

Refernces