3-methylbutane-1,2,3-tricarboxylic acid

Base Information

• Chemical Name: 3-methylbutane-1,2,3-tricarboxylic acid
• CAS No.: 77370-41-3
• Molecular Formula: C₈H₁₂O₆
• Molecular Weight: 204.18
• Mol file: 77370-41-3.mol

Synonyms:3-methylbutane-1,2,3-tricarboxylic acid

Chemical Property of 3-methylbutane-1,2,3-tricarboxylic acid

Chemical Property:

Purity/Quality:

98%min ^*data from raw suppliers

3-Methylbutane-1,2,3-tricarboxylicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-methylbutane-1,2,3-tricarboxylic acid

There total 36 articles about 3-methylbutane-1,2,3-tricarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 3-methylbutane-1,2,3-tricarboxylic acid (77370-41-3) + ozone (10028-15-6)

Guidance literature:

With acetic acid methyl ester; at 0 ℃; inactive α.α-dimethyl-tricarballyl acid;

Reference yield:

((3R,3aS,7R,8aS)-3,8,8-trimethyl-2,3,4,7,8,8a-hexahydro-1H-3a,7-cedaran-6-yl)methanol (21441-72-5) + acetone (67-64-1) → 3-methylbutane-1,2,3-tricarboxylic acid (77370-41-3) + 2,2-dimethylmalonic acid (595-46-0)

Guidance literature:

Erhitzen des Reaktionsprodukts mit wss. HNO₃;

DOI:10.1002/hlca.19420250624

Reference yield:

(-)-α-cedrene (469-61-4) + acetone (67-64-1) → 2,3,3-trimethylsuccinic acid (2103-16-4) + 3-methylbutane-1,2,3-tricarboxylic acid (77370-41-3) + succinic acid (110-15-6) + 2,2-dimethylmalonic acid (595-46-0)

Guidance literature:

anschliessend Behandeln mit wss. HNO₃ in Essigsaeure;

upstream raw materials:

2,2,3-trimethyl-3-cyclopentene-1-carboxylic acid

3-acetonyl-2,2-dimethyl-succinic acid

1,3,3-trimethyl-2-norbornanone

fenchone

Refernces

• 1、 Dette, Hans P.,Qi, Mian,Schroeder, David C.,Godt, Adelheid,Koop, Thomas. "Glass-forming properties of 3-methylbutane-1,2,3-tricarboxylic acid and its mixtures with water and pinonic acid". . p. 7024 - 7033. Retrieved 2014.