C₁₉H₃₀O₅

Base Information

• Chemical Name: C₁₉H₃₀O₅
• CAS No.: 371972-57-5
• Molecular Formula: C₁₉H₃₀O₅
• Molecular Weight: 338.444
• Mol file: 371972-57-5.mol

Synonyms:C₁₉H₃₀O₅

Chemical Property of C₁₉H₃₀O₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₉H₃₀O₅

There total 6 articles about C₁₉H₃₀O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

C19H28O5 → C19H30O5 (371972-57-5)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In ethyl acetate; for 3h; under 760.051 Torr;

DOI:10.1002/ejoc.201301727

Reference yield:

C17H30O6 (1606143-52-5) → C19H30O5 (371972-57-5)

Guidance literature:

Multi-step reaction with 5 steps

1.1: acetic acid; water / 0.5 h / 50 °C

2.1: 1H-imidazole; triphenylphosphine / tetrahydrofuran / 50 °C

2.2: 0.75 h / 50 °C

3.1: sodium hydroxide / methanol / 20 h / 20 °C

4.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 16 h / 20 °C / Inert atmosphere

4.2: 0.33 h / 20 °C

5.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 3 h / 760.05 Torr

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; palladium 10% on activated carbon; water; hydrogen; acetic acid; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; 4.1: |Cross Metathesis / 4.2: |Cross Metathesis;

DOI:10.1002/ejoc.201301727

Reference yield:

C14H26O6 (1606143-53-6) → C19H30O5 (371972-57-5)

Guidance literature:

Multi-step reaction with 4 steps

1.1: 1H-imidazole; triphenylphosphine / tetrahydrofuran / 50 °C

1.2: 0.75 h / 50 °C

2.1: sodium hydroxide / methanol / 20 h / 20 °C

3.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 16 h / 20 °C / Inert atmosphere

3.2: 0.33 h / 20 °C

4.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 3 h / 760.05 Torr

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; palladium 10% on activated carbon; hydrogen; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; 3.1: |Cross Metathesis / 3.2: |Cross Metathesis;

DOI:10.1002/ejoc.201301727

upstream raw materials:

C₁₆H₃₀O₁₀S₂

C₁₇H₃₀O₆

C₁₄H₂₆O₆

C₁₄H₂₄O₄

Downstream raw materials:

(3R,5S)-1-(4-hydroxy-3-methoxyphenyl)decane-3,5-diol

Refernces