Technology Process of C38H43N5O8
There total 5 articles about C38H43N5O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
benzaldehyde; H-Asp-Ala-Gly-OMe;
In
methanol;
at 20 ℃;
for 1h;
(9H-fluoren-9-yl)methyl (S)-1-isocyano-3-methylbutan-2-ylcarbamate;
In
methanol;
at 20 ℃;
for 50h;
optical yield given as %de;
diastereoselective reaction;
DOI:10.1016/j.tetlet.2011.08.090
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: Burgess Reagent / dichloromethane / 60 °C
2.1: methanol / 1 h / 20 °C
2.2: 50 h / 20 °C
With
Burgess Reagent;
In
methanol; dichloromethane;
2.1: Ugi reaction / 2.2: Ugi reaction;
DOI:10.1016/j.tetlet.2011.08.090
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 4-methyl-morpholine
2.1: toluene / 65 °C
3.1: dmap; formic acid / dichloromethane / -15 °C
4.1: Burgess Reagent / dichloromethane / 60 °C
5.1: methanol / 1 h / 20 °C
5.2: 50 h / 20 °C
With
4-methyl-morpholine; dmap; formic acid; Burgess Reagent;
In
methanol; dichloromethane; toluene;
5.1: Ugi reaction / 5.2: Ugi reaction;
DOI:10.1016/j.tetlet.2011.08.090