C₁₅H₁₃NO₂S

Base Information

• Chemical Name: C₁₅H₁₃NO₂S
• CAS No.: 145198-44-3
• Molecular Formula: C₁₅H₁₃NO₂S
• Molecular Weight: 271.34
• Mol file: 145198-44-3.mol

Synonyms:C₁₅H₁₃NO₂S

Chemical Property of C₁₅H₁₃NO₂S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅H₁₃NO₂S

There total 4 articles about C₁₅H₁₃NO₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

S-benzoylthiohydroxylamine (25740-80-1) + 4-methoxy-benzaldehyde (123-11-5) → C15H13NO2S (145198-44-3)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; Molecular sieve; Sealed tube;

DOI:10.1021/ol500385a

Reference yield:

C15H11NO3S (1571113-41-1) → C15H13NO2S (145198-44-3)

Guidance literature:

Multi-step reaction with 2 steps

1: water / acetonitrile; aq. phosphate buffer / 20 °C / pH 7.4

2: trifluoroacetic acid / dichloromethane / 20 °C / Molecular sieve; Sealed tube

With water; trifluoroacetic acid; In aq. phosphate buffer; dichloromethane; acetonitrile;

DOI:10.1021/ol500385a

Reference yield:

C12H15NOS (1571113-44-4) → C15H13NO2S (145198-44-3)

Guidance literature:

Multi-step reaction with 2 steps

1: water / acetonitrile; aq. phosphate buffer / 20 °C / pH 7.4

2: trifluoroacetic acid / dichloromethane / 20 °C / Molecular sieve; Sealed tube

With water; trifluoroacetic acid; In aq. phosphate buffer; dichloromethane; acetonitrile;

DOI:10.1021/ol500385a

upstream raw materials:

S-benzoylthiohydroxylamine

4-methoxy-benzaldehyde

C₁₄H₁₀FNOS

C₁₅H₁₁NO₃S

Downstream raw materials:

S-benzoylthiohydroxylamine

4-methoxy-benzaldehyde

C₁₅H₁₁NO₃S

C₁₂H₉NO₂S

Refernces