C₇₁H₅₀F₆N₂O₆

Base Information

• Chemical Name: C₇₁H₅₀F₆N₂O₆
• CAS No.: 1429193-80-5
• Molecular Formula: C₇₁H₅₀F₆N₂O₆
• Molecular Weight: 1141.18
• Mol file: 1429193-80-5.mol

Synonyms:C₇₁H₅₀F₆N₂O₆

Chemical Property of C₇₁H₅₀F₆N₂O₆

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₇₁H₅₀F₆N₂O₆

There total 3 articles about C₇₁H₅₀F₆N₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

N,N'-di(1-naphthyl)-N-phenyl-N'-(4-(hydroxymethyl)phenyl)benzidine (849146-79-8) + 3,5-bis(4-(1,2,2-trifluoroethenyloxy)benzyloxy)phenylacetic acid (1429193-79-2) → C71H50F6N2O6 (1429193-80-5)

Guidance literature:

With dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate; In tetrahydrofuran; dichloromethane; at 15 - 20 ℃; Inert atmosphere;

Reference yield:

4,4'-bis[N-(1-naphthyl)-N-phenylamino] biphenyl (123847-85-8) → C71H50F6N2O6 (1429193-80-5)

Guidance literature:

Multi-step reaction with 3 steps

1: trichlorophosphate / 1,2-dichloro-ethane / 7 h / 0 - 50 °C / Inert atmosphere

2: sodium tetrahydroborate; methanol / tetrahydrofuran / 24 h / 15 °C

3: 4-(dimethylamino)pyridinium tosylate; dicyclohexyl-carbodiimide / tetrahydrofuran; dichloromethane / 15 - 20 °C / Inert atmosphere

With methanol; sodium tetrahydroborate; dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate; trichlorophosphate; In tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane;

Reference yield:

C45H32N2O (847690-55-5) → C71H50F6N2O6 (1429193-80-5)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium tetrahydroborate; methanol / tetrahydrofuran / 24 h / 15 °C

2: 4-(dimethylamino)pyridinium tosylate; dicyclohexyl-carbodiimide / tetrahydrofuran; dichloromethane / 15 - 20 °C / Inert atmosphere

With methanol; sodium tetrahydroborate; dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate; In tetrahydrofuran; dichloromethane;

upstream raw materials:

4,4'-bis[N-(1-naphthyl)-N-phenylamino] biphenyl

C₄₅H₃₂N₂O

N,N'-di(1-naphthyl)-N-phenyl-N'-(4-(hydroxymethyl)phenyl)benzidine

3,5-bis(4-(1,2,2-trifluoroethenyloxy)benzyloxy)phenylacetic acid

Refernces