Technology Process of phosphonic acid dinonyl ester
There total 3 articles about phosphonic acid dinonyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
phosphorus tribromide;
In
diethyl ether;
at 0 - 25 ℃;
for 6h;
DOI:10.1002/cssc.202001551
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydroxide; potassium permanganate / water / 8 h / 50 °C
2: hydrogen; / hexane / 3 h / 250 °C / 30003 Torr
3: phosphorus tribromide / diethyl ether / 6 h / 0 - 25 °C
With
potassium permanganate; hydrogen; phosphorus tribromide; sodium hydroxide;
In
diethyl ether; hexane; water;
DOI:10.1002/cssc.202001551
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogen; / hexane / 3 h / 250 °C / 30003 Torr
2: phosphorus tribromide / diethyl ether / 6 h / 0 - 25 °C
With
hydrogen; phosphorus tribromide;
In
diethyl ether; hexane;
DOI:10.1002/cssc.202001551
