3-(BENZYLOXY)-4-METHOXYBENZALDEHYDE OXIME

Base Information

• Chemical Name: 3-(BENZYLOXY)-4-METHOXYBENZALDEHYDE OXIME
• CAS No.: 55667-17-9
• Molecular Formula: C15H15 N O3
• Molecular Weight: 257.289
• Hs Code.: 2928000090
• Mol file: 55667-17-9.mol

Synonyms:3-Benzyloxy-4-methoxybenzaldehydeoxime

Chemical Property of 3-(BENZYLOXY)-4-METHOXYBENZALDEHYDE OXIME

Chemical Property:

• Vapor Pressure: 4.05E-07mmHg at 25°C
• Boiling Point: 400.1°Cat760mmHg
• Flash Point: 195.8°C
• PSA: 51.05000
• Density: 1.11g/cm³
• LogP: 3.08230

Purity/Quality:

99% ^*data from raw suppliers

3-(BENZYLOXY)-4-METHOXYBENZALDEHYDE OXIME 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-(BENZYLOXY)-4-METHOXYBENZALDEHYDE OXIME

There total 2 articles about 3-(BENZYLOXY)-4-METHOXYBENZALDEHYDE OXIME which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.1%

3-benzyloxy-4-methoxybenzaldehyde (6346-05-0) → 3-benzyloxy-4-methoxybenzaldehyde oxime (55667-17-9)

Guidance literature:

With hydroxylamine hydrochloride; sodium acetate; In ethanol; for 1h; Heating;

Reference yield:

→ o-Benzylisovanillinoxim (55667-17-9)

Guidance literature:

d. entspr. Aldehyd, NH2OH*HCl;

Reference yield: 95.0%

3-benzyloxy-4-methoxybenzaldehyde oxime (55667-17-9) → 3-benzyloxy-4-methoxybenzonitrile (52805-37-5)

Guidance literature:

With phthalic anhydride; for 0.0833333h; Heating;

DOI:10.1002/jccs.200400093

upstream raw materials:

3-benzyloxy-4-methoxybenzaldehyde

Downstream raw materials:

3-benzyloxy-4-methoxy-benzylamine

3-benzyloxy-4-methoxybenzonitrile

3-benzyloxy-4-methoxybenzaldehyde

methyl 3-[3-(benzyloxy)-4-methoxyphenyl]-5-methyl-4,5-dihydroisoxazole-5-carboxylate

Refernces

• 1、 Wang, Eng-Chi,Huang, Keng-Shiang,Chen, Hsing-Ming,Wu, Chung-Chin,Lin, Gwo-Jiun. "An efficient method for the preparation of nitriles via the dehydration of aldoximes with phthalic anhydride". . p. 619 - 627. Retrieved 2007/10/03.