Technology Process of 1-hydroxy-2,3-dihydro-1H-inden-5-yl benzoate
There total 3 articles about 1-hydroxy-2,3-dihydro-1H-inden-5-yl benzoate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
borane-THF;
In
tetrahydrofuran;
at 0 - 20 ℃;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: boron tribromide / dichloromethane / -78 - 20 °C
1.2: 0.5 h
2.1: dmap; triethylamine / dichloromethane / 20 °C / Inert atmosphere
3.1: borane-THF / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
With
dmap; borane-THF; boron tribromide; triethylamine;
In
tetrahydrofuran; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: recombinant 5-hydroxymethylfurfural oxidase from Methylovorus sp. strain MP688; catalase from Micrococcus lysodeikticus; tris hydrochloride; D-Fructose; D-glucose / water; dimethyl sulfoxide / 24 h / 45 °C / pH 8.0 / Resolution of racemate; Enzymatic reaction
2: pyridine / dichloromethane / 20 °C
3: sodium tetrahydroborate; methanol
With
pyridine; methanol; sodium tetrahydroborate; D-Fructose; D-glucose; catalase from Micrococcus lysodeikticus; tris hydrochloride; recombinant 5-hydroxymethylfurfural oxidase from Methylovorus sp. strain MP688;
In
dichloromethane; water; dimethyl sulfoxide;
DOI:10.1080/10242422.2022.2038582