Technology Process of C39H48N5O8P
There total 5 articles about C39H48N5O8P which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
5-(ethylthio)-1H-tetrazole;
In
dichloromethane;
for 8h;
Inert atmosphere;
Molecular sieve;
DOI:10.1002/asia.201000828
- Guidance literature:
-
Multi-step reaction with 5 steps
1: palladium on activated charcoal; hydrogen / N,N-dimethyl-formamide / 24 h / 20 °C
2: benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / dichloromethane; N,N-dimethyl-formamide / 24 h / 20 °C
3: trifluoroacetic acid / tetrahydrofuran; water / 2 h / 5 °C
4: 2,6-di-tert-butyl-4-methylpyridine / dichloromethane; N,N-dimethyl-formamide / 0.83 h
5: 5-(ethylthio)-1H-tetrazole / dichloromethane / 8 h / Inert atmosphere; Molecular sieve
With
2,6-di-tert-butyl-4-methylpyridine; palladium on activated charcoal; hydrogen; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; 5-(ethylthio)-1H-tetrazole; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/asia.201000828
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 2,6-di-tert-butyl-4-methylpyridine / dichloromethane; N,N-dimethyl-formamide / 0.83 h
2: 5-(ethylthio)-1H-tetrazole / dichloromethane / 8 h / Inert atmosphere; Molecular sieve
With
2,6-di-tert-butyl-4-methylpyridine; 5-(ethylthio)-1H-tetrazole;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/asia.201000828
