2-DEOXYSTREPTAMINE, DIHYDROBROMIDE

Base Information

• Chemical Name: 2-DEOXYSTREPTAMINE, DIHYDROBROMIDE
• CAS No.: 84107-26-6
• Molecular Formula: 2BrH*C₆H₁₄N₂O₃
• Molecular Weight: 324.013
• Hs Code.: 2922190090
• Mol file: 84107-26-6.mol

Synonyms:2-deoxystreptamine dihydrobromide

Chemical Property of 2-DEOXYSTREPTAMINE, DIHYDROBROMIDE

Chemical Property:

• Storage Temp.: 2-8°C

Purity/Quality:

98%,99%, ^*data from raw suppliers

2-Deoxystreptamine dihydrobromide ^*data from reagent suppliers

Safty Information:

• Pictogram(s): 3692825
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26

MSDS Files:

SDS file from LookChem

Useful:

• Uses: An important component of several aminocyclitol antibiotics.

Technology Process of 2-DEOXYSTREPTAMINE, DIHYDROBROMIDE

There total 2 articles about 2-DEOXYSTREPTAMINE, DIHYDROBROMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

neomycin B trisulfate (4146-30-9,25389-98-4,28002-70-2,34289-38-8,92283-95-9) → 2-deoxystreptamine dihydrobromide (84107-26-6)

Guidance literature:

With water; hydrogen bromide; at 100 ℃; for 40h; Heating / reflux;

Reference yield: 59.0%

neomycin B (119-04-0) → 2-deoxystreptamine dihydrobromide (84107-26-6)

Guidance literature:

With hydrogen bromide; at 100 ℃; for 120h;

DOI:10.1016/j.carres.2013.03.019

Reference yield: 68.0%

2-deoxystreptamine dihydrobromide (84107-26-6) → (1α,2β,3α,4β,6β)-4,6-Diazido-1,2,3-cyclohexantriol (90899-14-2)

Guidance literature:

2-deoxystreptamine dihydrobromide; With sodium azide; potassium carbonate; trifluoroacetic anhydride; In dichloromethane; water; at 0 ℃; for 2h;

copper(II) sulfate; In dichloromethane; water; at 20 ℃; for 22h;

upstream raw materials:

neomycin B trisulfate

neomycin B

Downstream raw materials:

(1α,2β,3α,4β,6β)-4,6-Diazido-1,2,3-cyclohexantriol

(1α,2β,3α,4β,6β)-4,6-Diazido-1,2,3-cyclohexantriol-triacetat

Refernces

• 1、 -. "Antimicrobial 2-deoxystreptamine compounds". Page column 18-19. . Retrieved 2010/02/07.