HEXADECANOIC-15,15,16,16,16-D5 ACID

Base Information

• Chemical Name: HEXADECANOIC-15,15,16,16,16-D5 ACID
• CAS No.: 285979-77-3
• Molecular Formula: C₁₆H₃₂O₂
• Molecular Weight: 287.183
• Mol file: 285979-77-3.mol

Synonyms:HEXADECANOIC-15,15,16,16,16-D5 ACID;Hexadecanoic Acid-15,15,16,16,16-D5;Palmitic acid-15,15,16,16,16-d5

Chemical Property of HEXADECANOIC-15,15,16,16,16-D5 ACID

Chemical Property:

• Melting Point: 61-64 °C
• Boiling Point: 271.5 °C/100 mmHg(lit.)
• PSA: 37.30000
• Density: 0.868 g/mL at 25 °C
• LogP: 5.55230

Purity/Quality:

99% ^*data from raw suppliers

HexadecanoicAcid-15,15,16,16,16-d5 ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36
• Safety Statements: 26

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Hexadecanoic-15,15,16,16,16-d5 Acid (CAS# 285979-77-3) is a useful isotopically labeled research compound.

Technology Process of HEXADECANOIC-15,15,16,16,16-D5 ACID

There total 5 articles about HEXADECANOIC-15,15,16,16,16-D5 ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

1-hexadecylcarboxylic acid (57-10-3) → palmitic acid-d31 (39756-30-4,272442-14-5,285979-77-3,358730-99-1,78387-70-9,1219802-61-5)

Guidance literature:

1-hexadecylcarboxylic acid; With d8-isopropanol; 10% Pt/activated carbon; water-d2; at 120 ℃; for 24h;

With water; sodium hydroxide; at 70 ℃; for 24h; Reagent/catalyst;

DOI:10.1002/adsc.201600363

Reference yield:

β-lactoglobulin palmitic acid-2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,13,13,14,14,15,15,16,16,16-d31 1:1 complex → palmitic acid-d31 (39756-30-4,272442-14-5,285979-77-3,358730-99-1,78387-70-9,1219802-61-5) + β-lactoglobulin

Guidance literature:

In methanol; at 25 ℃; pH=8; Temperature; Time; Kinetics; aq. buffer;

DOI:10.1021/ja300092w

Reference yield:

β-lactoglobulin palmitic acid-9,9,10,10,11,11,12,12,13,13,14,14,15,15,16,16,16-d17 1:1 complex → palmitic acid-9,9,10,10,11,11,12,12,13,13,14,14,15,15,16,16,16-d17 (81462-28-4,272442-14-5,285979-77-3,358730-99-1,78387-70-9) + β-lactoglobulin

Guidance literature:

In methanol; at 25 ℃; pH=8; Temperature; Time; Kinetics; aq. buffer;

DOI:10.1021/ja300092w

upstream raw materials:

1-hexadecylcarboxylic acid

Downstream raw materials:

tripalmitin-d₉₃

d33-hexadecanethiol

[D₃₃]-hexadecyl bromide

1-hexadecyl-d33-ol

Refernces

• 1、 Liu, Lan,Michelsen, Klaus,Kitova, Elena N.,Schnier, Paul D.,Brown, Alex,Klassen, John S.. "Deuterium kinetic isotope effects on the dissociation of a protein-fatty acid complex in the gas phase". supporting information; scheme or table. p. 5931 - 5937. Retrieved 2012/05/07.