meta-Ar-CDM-COCl

Base Information

• Chemical Name: meta-Ar-CDM-COCl
• CAS No.: 1416319-77-1
• Molecular Formula: C₁₂H₇ClO₄
• Molecular Weight: 250.638
• Mol file: 1416319-77-1.mol

Synonyms:meta-Ar-CDM-COCl

Chemical Property of meta-Ar-CDM-COCl

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of meta-Ar-CDM-COCl

There total 4 articles about meta-Ar-CDM-COCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

meta-Ar-CDM-CO2H (1416319-76-0) → meta-Ar-CDM-COCl (1416319-77-1)

Guidance literature:

With oxalyl dichloride; In dichloromethane; at 20 ℃; for 17h;

Reference yield:

3-carboxymethyl-benzoic acid (2084-13-1) → meta-Ar-CDM-COCl (1416319-77-1)

Guidance literature:

Multi-step reaction with 2 steps

1.1: acetic anhydride / 0.33 h / 120 °C

1.2: 17 h / 20 °C

1.3: pH 1

2.1: oxalyl dichloride / dichloromethane / 17 h / 20 °C

With oxalyl dichloride; acetic anhydride; In dichloromethane;

Reference yield:

3-methoxycarbonylbenzyl bromide (1129-28-8) → meta-Ar-CDM-COCl (1416319-77-1)

Guidance literature:

Multi-step reaction with 4 steps

1.1: ethanol; water / 2 h / 65 °C

2.1: water; sulfuric acid / 3 h / 160 °C

3.1: acetic anhydride / 0.33 h / 120 °C

3.2: 17 h / 20 °C

3.3: pH 1

4.1: oxalyl dichloride / dichloromethane / 17 h / 20 °C

With oxalyl dichloride; sulfuric acid; water; acetic anhydride; In ethanol; dichloromethane; water;

upstream raw materials:

3-methoxycarbonylbenzyl bromide

methyl 3-cyanomethylbenzoate

3-carboxymethyl-benzoic acid

meta-Ar-CDM-CO₂H

Refernces