Technology Process of PHENYLSULFONYLMETHYL ISOCYANIDE
There total 5 articles about PHENYLSULFONYLMETHYL ISOCYANIDE which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
diisopropylamine; trichlorophosphate;
In
tetrahydrofuran; acetonitrile;
at -20 - 5 ℃;
for 1h;
Inert atmosphere;
DOI:10.1002/ejoc.201403615
- Guidance literature:
-
Multi-step reaction with 2 steps
1: formic acid; toluene / 3 h / 100 °C / Inert atmosphere; Microwave irradiation
2: diisopropylamine; trichlorophosphate / tetrahydrofuran; acetonitrile / 1 h / -20 - 5 °C / Inert atmosphere
With
diisopropylamine; trichlorophosphate;
In
tetrahydrofuran; formic acid; toluene; acetonitrile;
DOI:10.1002/ejoc.201403615
- Guidance literature:
-
Multi-step reaction with 3 steps
1: N-Bromosuccinimide / dichloromethane / 1 h / 0 °C
2: formic acid; toluene / 3 h / 100 °C / Inert atmosphere; Microwave irradiation
3: diisopropylamine; trichlorophosphate / tetrahydrofuran; acetonitrile / 1 h / -20 - 5 °C / Inert atmosphere
With
N-Bromosuccinimide; diisopropylamine; trichlorophosphate;
In
tetrahydrofuran; formic acid; dichloromethane; toluene; acetonitrile;
DOI:10.1002/ejoc.201403615
