CH₃OOCCH₂CH(CH₂HgBr)CH(OOCCF₃)CH₂CH₂CH₂CH₃

Base Information

• Chemical Name: CH₃OOCCH₂CH(CH₂HgBr)CH(OOCCF₃)CH₂CH₂CH₂CH₃
• CAS No.: 87434-00-2
• Molecular Formula: C₁₂H₁₈BrF₃HgO₄
• Molecular Weight: 563.762
• Mol file: 87434-00-2.mol

Synonyms:CH₃OOCCH₂CH(CH₂HgBr)CH(OOCCF₃)CH₂CH₂CH₂CH₃

Chemical Property of CH₃OOCCH₂CH(CH₂HgBr)CH(OOCCF₃)CH₂CH₂CH₂CH₃

Chemical Property:

Purity/Quality:

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Technology Process of CH₃OOCCH₂CH(CH₂HgBr)CH(OOCCF₃)CH₂CH₂CH₂CH₃

There total 1 articles about CH₃OOCCH₂CH(CH₂HgBr)CH(OOCCF₃)CH₂CH₂CH₂CH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

mercury(II) trifluoroacetate (13257-51-7) + trans-5-n-butyl-4-methyl-4,5-dihydro-2(3H)-furanone (87433-77-0,99530-35-5,39212-23-2,39638-67-0,55013-32-6,80041-00-5,80041-01-6,89163-43-9,105015-53-0,105119-22-0) → C4H4O2(CH2HgBr)(CH2CH2CH2CH3) (87433-99-6) + CH3OOCCH2CH(CH2HgBr)CH(OOCCF3)CH2CH2CH2CH3 (87434-00-2)

Guidance literature:

With potassium bromide; In tetrachloromethane; water; soln. of carboxylic acid ester and mercury salt in org. solvent stood at 25 °C for 19 h, satd. aq. KBr added, stirred for 0.5 h; laeyrs sepd., aq. phase extd. with CHCl3, combined org. layers dried, concd. in vac., chromd. (EtOAc-hexane);

DOI:10.1021/ja00361a024

upstream raw materials:

mercury(II) trifluoroacetate

trans-5-n-butyl-4-methyl-4,5-dihydro-2(3H)-furanone