1-(4-Bromobutoxy)-4-methoxybenzene

Base Information

• Chemical Name: 1-(4-Bromobutoxy)-4-methoxybenzene
• CAS No.: 2033-83-2
• Molecular Formula: C11H15BrO2
• Molecular Weight: 259.143
• Hs Code.: 2909309090
• European Community (EC) Number: 675-181-8
• DSSTox Substance ID: DTXSID90366309
• Wikidata: Q82151454
• Mol file: 2033-83-2.mol

Synonyms:1-(4-Bromobutoxy)-4-methoxybenzene;2033-83-2;1-(4-bromobutoxy)-4-methoxy-benzene;MFCD00980264;SCHEMBL7823783;4-(4-methoxyphenoxy)butylbromide;DTXSID90366309;XNMUBVHIMDDDNF-UHFFFAOYSA-N;1-(4-methoxyphenoxy)-4-bromobutane;AKOS000343611;FS-4657;CS-0333674;FT-0742340;A814465;J-013227

Chemical Property of 1-(4-Bromobutoxy)-4-methoxybenzene

Chemical Property:

• Appearance/Colour: low-melting solid
• Vapor Pressure: 0.000229mmHg at 25°C
• Refractive Index: 1.524
• Boiling Point: 335.7 °C at 760 mmHg
• Flash Point: 146.6 °C
• PSA: 18.46000
• Density: 1.294 g/cm³
• LogP: 3.24910
• XLogP3: 3.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 6
• Exact Mass: 258.02554
• Heavy Atom Count: 14
• Complexity: 133

Purity/Quality:

99.0%Min ^*data from raw suppliers

1-(4-Bromobutoxy)-4-methoxybenzene 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC=C(C=C1)OCCCCBr

Technology Process of 1-(4-Bromobutoxy)-4-methoxybenzene

There total 5 articles about 1-(4-Bromobutoxy)-4-methoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1,4-dibromo-butane (110-52-1) + 4-methoxy-phenol (150-76-5) → 1-(4-methoxyphenoxy)-4-bromobutane (2033-83-2)

Guidance literature:

With potassium carbonate; potassium iodide; In acetone; for 48h; Reflux;

DOI:10.1039/d0nj02524k

Reference yield: 82.0%

4-methoxy-phenol (150-76-5) → 1,4-dibromo-butane (110-52-1) + 1-(4-methoxyphenoxy)-4-bromobutane (2033-83-2)

Guidance literature:

Reference yield:

4-methoxy-phenol (150-76-5) → 1-(4-methoxyphenoxy)-4-bromobutane (2033-83-2)

Guidance literature:

With potassium carbonate; In acetone;

DOI:10.1007/s10600-013-0585-1

upstream raw materials:

1,4-dibromo-butane

4-methoxy-phenol

sodium 4-methoxyphenolate

Downstream raw materials:

3-<ω-(4-Methoxyphenoxy)butyl>thiophene

1-(but-3-en-1-yloxy)-4-methoxybenzene

9-O-[3-(4-methyl-phenoxy)butyl]berberine bromide

1-[4-(4-Methoxy-phenoxy)-butyl]-3,7-dimethyl-3,7-dihydro-purine-2,6-dione

Refernces

• 1、 Selivanova,Maiorova,Shklyaeva,Abashev. "Synthesis of push-pull chromophores including an N-[4-(4-methoxyphenoxy)butyl]carbazole fragment". . p. 735 - 739. Retrieved 2015.
• 2、 Wei, Tai-Bao,Qi, Li-Hua,Zhang, Qin-Peng,Zhang, Wen-Huan,Yao, Hong,Zhang, You-Ming,Lin, Qi. "Stimuli-responsive supramolecular polymer network based on bi-pillar[5]arene for efficient adsorption of multiple organic dye contaminants". . p. 12531 - 12537. Retrieved 2020.
• 3、 Chen, Zelong,Hu, Xianjun,Jin, Ming,Pei, Yuxin,Pei, Zhichao,Pu, Liang,Wang, Yang. "Tumor microenvironment responsive supramolecular glyco-nanovesicles based on diselenium-bridged pillar[5]arene dimer for targeted chemotherapy". supporting information. p. 10642 - 10645. Retrieved 2020/10/02.