butyl-di-t-butylchlorophosphonium bromide

Base Information

• Chemical Name: butyl-di-t-butylchlorophosphonium bromide
• CAS No.: 81193-50-2
• Molecular Formula: Br*C₁₂H₂₇ClP
• Molecular Weight: 317.677
• Mol file: 81193-50-2.mol

Synonyms:butyl-di-t-butylchlorophosphonium bromide

Chemical Property of butyl-di-t-butylchlorophosphonium bromide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of butyl-di-t-butylchlorophosphonium bromide

There total 2 articles about butyl-di-t-butylchlorophosphonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

di(tert-butyl)(n-butyl)phosphine (29949-72-2) → Bromoform (75-25-2) + butyl-di-t-butylchlorophosphonium bromide (81193-50-2)

Guidance literature:

With carbon tetrabromide; hydrogen chloride; In diethyl ether; 1) -120 deg C to -50 deg C 2) 0 deg C, Et₂O;

Reference yield: 60.0%

butyl-di-t-butylbromophosphonium tribromomethanid (81193-49-9) → tribromo(2H)methane (2909-52-6) + butyl-di-t-butylchlorophosphonium bromide (81193-50-2)

Guidance literature:

With hydrogenchloride; In diethyl ether; -120 deg C to r.t.;

upstream raw materials:

di(tert-butyl)(n-butyl)phosphine

butyl-di-t-butylbromophosphonium tribromomethanid

Refernces