β-methyl-3-chlorostyrene

Base Information

• Chemical Name: β-methyl-3-chlorostyrene
• CAS No.: 26293-11-8
• Molecular Formula: C₉H₉Cl
• Molecular Weight: 152.623
• Mol file: 26293-11-8.mol

Synonyms:β-methyl-3-chlorostyrene

Chemical Property of β-methyl-3-chlorostyrene

Chemical Property:

Purity/Quality:

98% HPLC ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of β-methyl-3-chlorostyrene

There total 2 articles about β-methyl-3-chlorostyrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-chloro-3-(prop-1-yn-1-yl)benzene (43136-84-1) → β-methyl-3-chlorostyrene (26293-11-8)

Guidance literature:

With hydrogen; In hexane;

DOI:10.1002/cjoc.202100252

Reference yield:

m-chlorophenylacetylene (766-83-6) → β-methyl-3-chlorostyrene (26293-11-8)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydride / 1,4-dioxane

2: hydrogen / hexane

With hydrogen; sodium hydride; In 1,4-dioxane; hexane;

DOI:10.1002/cjoc.202100252

Reference yield: 95.0%

β-methyl-3-chlorostyrene (26293-11-8) → C9H10Cl2 (408317-90-8)

Guidance literature:

With 4-Methoxybenzenethiol; 10-methyl-9-(2,4,6-trimethylphenyl) acridinium tetrafluoroborate; 2,6-lutidine hydrochloride; In chloroform; 2,2,2-trifluoroethanol; for 16h; Irradiation; Inert atmosphere;

DOI:10.1038/nchem.2000

upstream raw materials:

1-chloro-3-(prop-1-yn-1-yl)benzene

m-chlorophenylacetylene

Downstream raw materials:

C₉H₁₀Cl₂

2-bromo-3'-chloropropiophenone

bupropion

Refernces