2-(2-butoxyethoxy)ethyl 4-methylbenzenesulfonate

Base Information

• Chemical Name: 2-(2-butoxyethoxy)ethyl 4-methylbenzenesulfonate
• CAS No.: 50964-16-4
• Molecular Formula: C15H24 O5 S
• Molecular Weight: 316.419
• Mol file: 50964-16-4.mol

Synonyms:Ethanol,2-(2-butoxyethoxy)-, 4-methylbenzenesulfonate (9CI); 3,6-Dioxadecyl tosylate;NSC 406347

Chemical Property of 2-(2-butoxyethoxy)ethyl 4-methylbenzenesulfonate

Chemical Property:

• Vapor Pressure: 3.24E-07mmHg at 25°C
• Boiling Point: 430.5°Cat760mmHg
• Flash Point: 214.2°C
• Density: 1.121g/cm³

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(2-butoxyethoxy)ethyl 4-methylbenzenesulfonate

There total 1 articles about 2-(2-butoxyethoxy)ethyl 4-methylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

Diethylene glycol monobutyl ether (112-34-5,9004-77-7) + p-toluenesulfonyl chloride (98-59-9) → diethylene glycol monobutyl ether tosylate (50964-16-4)

Guidance literature:

Diethylene glycol monobutyl ether; p-toluenesulfonyl chloride; With dmap; In dichloromethane; at 20 ℃;

With triethylamine; In dichloromethane; at 20 ℃;

DOI:10.1021/jo102358d

Reference yield: 56.0%

1,1,3,3,5,5-hexakis(4-(hydroxymethyl)phenoxy)cyclotriphosphazene (49864-98-4) + diethylene glycol monobutyl ether tosylate (50964-16-4) → hexakiscyclophosphazene

Guidance literature:

With sodium hydride; In tetrahydrofuran; for 48h; Heating;

Reference yield:

diethylene glycol monobutyl ether tosylate (50964-16-4) + syringic aldehyde (134-96-3) → 4-[2-(2-butoxy-ethoxy)-ethoxy]-3,5-dimethoxy-benzaldehyde (300848-88-8)

Guidance literature:

With sodium carbonate; potassium iodide; In N,N-dimethyl-formamide; at 60 - 70 ℃;

DOI:10.1039/b000827n

upstream raw materials:

Diethylene glycol monobutyl ether

p-toluenesulfonyl chloride

Downstream raw materials:

3-Jod-5-butoxycarbonyl-benzoesaeure-<2-(2-butoxy-aethoxy)-aethylester>

3-Jod-5-pentyloxycarbonyl-benzoesaeure-<2-(2-butoxy-aethoxy)-aethylester>

3-Jod-5-<2-(2-aethoxy-aethoxy)-aethoxy-carbonyl>-benzoesaeure-<2-(2-butoxy-aethoxy)-aethylester>

(4-Acetamino-2-propionyl-phenyl)-<2-(2-butyloxy-ethoxy)-ethyl>-ether

Refernces

• 1、 Harjani, Jitendra R.,Liang, Chen,Jessop, Philip G.. "A Synthesis of acetamidines". experimental part. p. 1683 - 1691. Retrieved 2011/05/12.
• 2、 Podda, Gianni. "STUDIES ON CYCLOPHOSPHAZENES. II. SYNTHESIS AND CATALYTIC ACTIVITY OF NEW TYPES OF HEXA-SUBSTITUTED CYCLOPHOSPHAZENIC PODANDS". . p. 397 - 400. Retrieved 2007/10/02.