N-(2-METHOXYETHYL)ETHYLAMINE

Base Information

• Chemical Name: N-(2-METHOXYETHYL)ETHYLAMINE
• CAS No.: 34322-82-2
• Molecular Formula: C5H13 N O
• Molecular Weight: 103.164
• Hs Code.: 2922199090
• Mol file: 34322-82-2.mol

Synonyms:Diethylamine,2-methoxy- (8CI); (2-Methoxyethyl)ethylamine; 2-Methoxydiethylamine;Ethyl(2-methoxyethyl)amine; N-(2-Methoxyethyl)ethanamine;N-(2-Methoxyethyl)ethylamine; N-Ethyl-2-methoxyethanamine;N-Ethyl-2-methoxyethylamine; N-Ethyl-N-(2-methoxyethyl)amine

Chemical Property of N-(2-METHOXYETHYL)ETHYLAMINE

Chemical Property:

• Vapor Pressure: 34mmHg at 25°C
• Refractive Index: 1.399
• Boiling Point: 102.2°Cat760mmHg
• Flash Point: 28.2°C
• PSA: 21.26000
• Density: 0.817g/cm³
• LogP: 0.63320

Purity/Quality:

98%,99%, ^*data from raw suppliers

N-(2-Methoxyethyl)ethylamine ^*data from reagent suppliers

Safty Information:

• Statements: 10-34-41-37/38-22
• Safety Statements: 26-36/37/39-39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-(2-METHOXYETHYL)ETHYLAMINE

There total 7 articles about N-(2-METHOXYETHYL)ETHYLAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

N-(2-methoxyethyl)acetamide (5417-42-5) → N-ethyl-2-methoxyethanamine (34322-82-2)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; Heating;

DOI:10.1021/ja00363a007

Reference yield:

acetaldehyde (75-07-0,9002-91-9) + 2-methoxyethylamine (109-85-3) → N-ethyl-2-methoxyethanamine (34322-82-2)

Guidance literature:

With potassium hydroxide; dipotassium hydrogenphosphate; phosphoric acid; at 10 - 12 ℃; for 4h; Yield given; electrochemical reductive amination, lead cathode, current density 0.05 A/cm², pH 12;

Reference yield:

ethylamine (75-04-7,85404-22-4) + 2-Bromoethyl methyl ether (6482-24-2) → N-ethyl-2-methoxyethanamine (34322-82-2)

Guidance literature:

With sodium hydroxide;

upstream raw materials:

N-ethyl-N-(2-methoxyethyl)aniline

ethylamine

2-Bromoethyl methyl ether

N-(2-methoxyethyl)acetamide

Downstream raw materials:

N-ethyl-N-(2-methoxyethyl)acetamide

N-ethyl-N-(2-methoxy-ethyl)-2-methyl-5-nitro-N'-(2,4,6-trimethyl-phenyl)-pyrimidine-4,6-diamine

N-{5-chloro-2-[ethyl(2-methoxyethyl)amino]phenyl}-N'-(5-cyano-2-pyrazinyl)urea

8-(4-Benzyloxy-phenyl)-7-oxo-7H-thieno[2,3-a]quinolizine-10-carboxylic acid ethyl-(2-methoxy-ethyl)-amide

Refernces

• 1、 Smirnov, Yu. D.,Pavlichenko, V. F.,Tomilov, A. P.. "ELECTROCHEMICAL REDUCTIVE AMINATION. II. AMINATION OF ALIPHATIC ALDEHYDES WITH PRIMARY AMINES". . p. 374 - 380. Retrieved 2007/10/02.