C₁₅H₂₀O

Base Information

• Chemical Name: C₁₅H₂₀O
• CAS No.: 1055197-69-7
• Molecular Formula: C₁₅H₂₀O
• Molecular Weight: 216.323
• Mol file: 1055197-69-7.mol

Synonyms:C₁₅H₂₀O

Chemical Property of C₁₅H₂₀O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅H₂₀O

There total 1 articles about C₁₅H₂₀O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2,6-dimethyl-4-tert-butylphenol (879-97-0) + propargyl bromide (106-96-7) → C15H20O (1055197-69-7)

Guidance literature:

2,6-dimethyl-4-tert-butylphenol; With potassium carbonate; In acetone; for 1h; Reflux;

propargyl bromide; In acetone; for 17h; Reflux;

DOI:10.1002/asia.201600202

Reference yield: 87.0%

C15H20O (1055197-69-7) + 9,10-bis(azidomethyl)anthracene (753024-99-6) → C46H52N6O2

Guidance literature:

With copper(l) iodide; In tetrahydrofuran; water; for 15h; Reflux;

DOI:10.1002/asia.201600202

Reference yield: 81.0%

C15H20O (1055197-69-7) + 9-(azidomethyl)anthracene (195133-98-3) → C30H31N3O

Guidance literature:

With copper(l) iodide; In tetrahydrofuran; water; at 65 ℃;

DOI:10.1016/j.tet.2016.06.055

upstream raw materials:

2,6-dimethyl-4-tert-butylphenol

propargyl bromide

Downstream raw materials:

C₃₀H₂₈ClNO₂

Refernces

• 1、 Zhao, Jiang-Lin,Wu, Chong,Tomiyasu, Hirotsugu,Zeng, Xi,Elsegood, Mark R. J.,Redshaw, Carl,Yamato, Takehiko. "A Rare and Exclusive Endoperoxide Photoproduct Derived from a Thiacalix[4]arene Crown-Shaped Derivative Bearing a 9,10-Substituted Anthracene Moiety". . p. 1606 - 1612. Retrieved 2016/06/01.