C₂₈H₂₉NO₁₅

Base Information

• Chemical Name: C₂₈H₂₉NO₁₅
• CAS No.: 1432474-27-5
• Molecular Formula: C₂₈H₂₉NO₁₅
• Molecular Weight: 619.536
• Mol file: 1432474-27-5.mol

Synonyms:C₂₈H₂₉NO₁₅

Chemical Property of C₂₈H₂₉NO₁₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₈H₂₉NO₁₅

There total 3 articles about C₂₈H₂₉NO₁₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C32H37NO15 (1432474-22-0) → C28H29NO15 (1432474-27-5)

Guidance literature:

With trifluoroacetic acid; at 0 - 20 ℃;

DOI:10.1016/j.cclet.2013.02.003

Reference yield:

L-valine tert-butylester hydrochloride (13518-40-6) → C28H29NO15 (1432474-27-5)

Guidance literature:

Multi-step reaction with 3 steps

1.1: pyridine / dichloromethane / 0.25 h / -10 °C / Inert atmosphere

1.2: 2 h / -10 °C / Inert atmosphere

2.1: triethylamine / tetrahydrofuran; N,N-dimethyl-formamide / 10 h / 50 °C / Inert atmosphere

3.1: trifluoroacetic acid / 0 - 20 °C

With pyridine; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/j.cclet.2013.02.003

Reference yield:

valine tert-butyl ester isocyanate → C28H29NO15 (1432474-27-5)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran; N,N-dimethyl-formamide / 10 h / 50 °C / Inert atmosphere

2: trifluoroacetic acid / 0 - 20 °C

With triethylamine; trifluoroacetic acid; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1016/j.cclet.2013.02.003

upstream raw materials:

C₃₂H₃₇NO₁₅

L-valine tert-butylester hydrochloride

Downstream raw materials:

scutellarin

Refernces

• 1、 Jiang, Feng-Jie,Fu, Xiao-Zhong,Wang, Shan-Wu,Huang, Yong,Zhou, Wen,Wang, Ai-Min,Wang, Yong-Lin. "Synthesis and physiochemical property evaluation of carbamate derivatives of scutellarin methyl ester". . p. 338 - 340. Retrieved 2013/06/26.